A hydraulic oil composition
A technology of hydraulic oil composition and polymer, applied in the direction of lubricating composition, petroleum industry, etc., can solve the problem of easy generation of precipitates, etc., and achieve the effect of excellent biodegradability and excellent emulsification resistance
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[0081] Hereinafter, the present invention will be described in more detail with reference to Examples and Comparative Examples.
[0082] [Synthesis of Ester Mixture I]
[0083] Put 1200g (8.94mol) of trimethylolpropane (TMP) and 2486g (8.94mol) of industrial oleic acid manufactured by NOF Co. NAA-34 (unsaturated acid content: 90% by mass) was reacted under normal pressure at 220° C. while distilling off the reaction water under a nitrogen stream until the acid value was 0.1 mgKOH / g or less. After cooling the reaction, it was filtered to remove most of the unreacted trimethylolpropane. Then, about 2500 g of partial ester I are obtained by distillation.
[0084] The obtained partial ester I was silylated (TMSized), and then analyzed by gas chromatography under the following conditions. It was a partial ester mixture of 98.1% by mass of TMP monoester and 1.9% by mass of TMP diester.
[0085]
[0086] Column: packed column OV-1 (0.4m)
[0087] Heating conditions: from 150°C ...
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