Finishing application of aminophenylsilsesquioxane tussah silk textile and modified finishing textile or fabric

A technology of silsesquioxane and aminophenyl, which is applied in fiber treatment, animal fiber, textile and paper making, etc.

Active Publication Date: 2016-05-25
EASTERN LIAONING UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Up to now, there is no public technical record about cage silsesquioxane, especially aminophenyl cage silsesquioxane as textile fiber material or its fabric modification finishing material and method in the prior art

Method used

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  • Finishing application of aminophenylsilsesquioxane tussah silk textile and modified finishing textile or fabric
  • Finishing application of aminophenylsilsesquioxane tussah silk textile and modified finishing textile or fabric
  • Finishing application of aminophenylsilsesquioxane tussah silk textile and modified finishing textile or fabric

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] (1) Obtain a finishing solution containing aminophenylsilsesquioxane OAPS

[0020] Add OAPS into tetrahydrofuran and dissolve to obtain an OAPS solution with a concentration of 5.0 g / L. Add water to dilute the OAPS solution to obtain an OAPS aqueous solution with a concentration of 1.0 g / L. Take 10 ml of the OAPS aqueous solution and add 0.1 g of 1,4-butanediol to shrink Glyceryl ether and 0.05g sodium methylene dinaphthalene sulfonate diffusing agent, then add 90ml water to obtain 100ml finishing solution containing aminophenylsilsesquioxane OAPS;

[0021] (2) Modification and finishing of tussah silk

[0022] Immerse 2g of tussah silk into the finishing liquid prepared in step (1) at 40°C, raise the temperature to 60°C for 45 minutes, take out the finished tussah silk fabric, wash and dry it, and obtain the tussah silk raw material and its fabric modified finishing fabric .

Embodiment 2

[0024] (1) Obtain a finishing solution containing aminophenylsilsesquioxane OAPS

[0025] Add OAPS to tetrahydrofuran to dissolve to obtain an OAPS solution with a concentration of 10g / L, add water to dilute the OAPS solution to obtain an OAPS aqueous solution with a concentration of 2.0g / L, take 10ml of the OAPS aqueous solution, and add 0.2g of 1,4-butanediol Glycidyl ether BDGE and 0.1g sodium methylene dinaphthalene sulfonate diffusing agent, then add 90ml water to make 100ml finishing solution containing aminophenylsilsesquioxane OAPS;

[0026] (2) Modification and finishing of tussah silk

[0027] Immerse 2g of tussah silk into the finishing liquid prepared in step (1) at 40°C, raise the temperature to 70°C, and finish at this temperature for 60 minutes, take out the finished tussah silk fabric, wash, and dry to obtain the tussah silk raw material and its fabric Modified finishing fabric.

Embodiment 3

[0029] (1) Obtain a finishing solution containing aminophenylsilsesquioxane OAPS

[0030] Add OAPS to tetrahydrofuran to dissolve to obtain an OAPS solution with a concentration of 15g / L, add water to dilute the OAPS solution to obtain an OAPS aqueous solution with a concentration of 3.0g / L, take 10ml of the OAPS aqueous solution, and add 0.3g of 1,4-butanediol glycidol Ether BDGE and 0.15g sodium methylene dinaphthalene sulfonate diffusing agent, then add 90ml water to obtain 100ml aminophenyl silsesquioxane finishing solution;

[0031] (2) Modification and finishing of tussah silk

[0032] Immerse 2g of tussah silk fabric in the above finishing solution at 40°C, raise the temperature to 85°C, and finish at this temperature for 45 minutes, take out the finished tussah silk fabric, wash, and dry to obtain the tussah silk raw material and its fabric modified finishing fabric.

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Abstract

The invention provides finishing application of an aminophenylsilsesquioxane tussah silk textile and a modified finishing textile or fabric. The finishing application is characterized in that an aminophenylsilsesquioxane water solution is mixed with 1,4-butanediol glycidyl ether and disodium methylenebisnaphthalenesulphonate to obtain finishing liquid for carrying out modified finishing on tussah silk, so as to prepare the tussah silk textile modified finishing textile or fabric. The textile or fabric has good anti-ultraviolet, crease-resisting and water-repelling properties of tussah silk fibers.

Description

technical field [0001] The application of the present invention relates to the technical field of fabric modification, in particular to the technical field of finishing modification application of tussah silk materials and fabrics thereof. Background technique [0002] Tussah silk has natural color, soft touch, strong acid and alkali resistance, and good comfort. It is an excellent natural textile raw material. However, tussah silk fabrics also have technical problems such as anti-wrinkle ability and unsatisfactory anti-ultraviolet ability. To this end, technical R&D personnel have developed various finishing and modification technical solutions. Tussah silk materials and their fabrics are endowed with unique functions, such as anti-ultraviolet function, antibacterial function and anti-wrinkle performance, to meet the special functions of consumers or special industries. The use requirements, especially to meet the application technology requirements of some high-end clothin...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/643D06M13/165D06M13/256D06M101/12
CPCD06M13/165D06M13/256D06M15/643D06M2101/12
Inventor 路艳华郝旭程德红尹丽馨林杰王勃翔李佳
Owner EASTERN LIAONING UNIV
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