Element-processing layered structure, method for manufacturing element-processing layered structure, and method for manufacturing thin element using same
A manufacturing method and laminated body technology, applied in semiconductor/solid-state device manufacturing, electrical components, chemical instruments and methods, etc., can solve problems such as reduced adhesion, melting of solder bumps, inability to peel off, etc., and achieve the effect of improving productivity
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[0082] Example
[0083] The following examples are given to illustrate the present invention, but the present invention is not limited by these examples. The evaluation methods of the glass transition temperature, weight loss rate, and adhesion will be described.
[0084] (1) Measurement of glass transition temperature
[0085] Using a bar coater, apply the heat-resistant resin solution (B1 to B9, A1 to A6) described in the following production examples 1 to 15 to the glossy surface of the 18 μm thick electrolytic copper foil so that the thickness becomes 20 μm Then, it was dried at 80°C for 10 minutes, at 150°C for 10 minutes, and then heated at 250°C for 10 minutes in a nitrogen atmosphere to convert it into polyimide to obtain a resin-laminated copper foil. Next, the entire surface of the copper foil in the obtained resin-laminated copper foil was etched with a ferric chloride solution to obtain a single film of heat-resistant resin.
[0086] About 10 mg of the obtained single fi...
Example Embodiment
[0119] Production example 1 (polymerization of heat-resistant resin B solution)
[0120] Into a reactor equipped with a thermometer, a dry nitrogen inlet, a heating and cooling device using warm water and cooling water, and a stirring device, together with 2264g of NMP, 75.7g (0.7mol) of PDA and 60.1g (0.3 mol) DAE, after dissolving, add 176.5g (0.6mol) BPDA and 87.2g (0.4mol) PMDA, react at room temperature for 1 hour, and then at 60°C for 5 hours to obtain 15% by weight polyamic acid resin solution (B-1).
Example
[0121] Production examples 2-7 (polymerization of heat-resistant resin B solution)
[0122] Except changing the type and amount of acid dianhydride and diamine as shown in Table 1, the same operation as in Production Example 1 was performed to obtain a 15% by weight polyamic acid resin solution (B-2~ 7).
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