Corn stalk-flax gum synthetic light coupling coagulant aid
A technology of corn stalks and flax gum, which is applied in solid waste removal, flocculation/sedimentation water/sewage treatment, water/sludge/sewage treatment, etc., can solve the problems of easy generation of dust and secondary pollution, and achieve a good society. Benefit, environmental protection, and the effect of material and energy recycling
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Embodiment 1
[0009] Take the ground and pulverized corn stalks, heat to 60°C in a mixed solution of 1.5 mol / L ethylene glycol and 2.0 mol / L sodium hydroxide with a volume ratio of 1:3, soak for 6 hours, and then take the filtrate and filter residue for later use; then the filtrate , flax glue, catalyst and filter residue were injected into the hydrothermal synthesis reaction kettle according to the mass percentage of 40%, 28%, 5% and 27%, heated to 115°C, reacted at 1.5MPa for 4h, cooled to room temperature, and took the upper layer The liquid is concentrated and precipitated, and the precipitate is dried at 40°C to obtain a light coupling coagulant solid. The catalyst is trialkyl ammonium chloride.
Embodiment 2
[0011] Take the ground and pulverized corn stalks, heat to 65°C in a mixed solution of 2.0mol / L ethylene glycol and 2.5mol / L sodium hydroxide with a volume ratio of 2:3, soak for 7 hours, and then take the filtrate and filter residue for later use; then the filtrate , flax glue, catalyst and filter residue were injected into the hydrothermal synthesis reaction kettle according to the mass percentage of 41%, 25%, 6% and 28%, heated to 120°C, reacted at 2.0MPa for 5h, cooled to room temperature, and took the upper layer The liquid is concentrated and precipitated, and the precipitate is dried at 45°C to obtain a light coupling coagulant solid. The catalyst is dodecyltrimethylammonium chloride.
Embodiment 3
[0013] Take the ground and pulverized corn stalks, heat to 70°C in a mixed solution of 2.5 mol / L ethylene glycol and 3.0 mol / L sodium hydroxide with a volume ratio of 1:2, soak for 8 hours, then take the filtrate and filter residue for later use; then the filtrate , flax glue, catalyst and filter residue were injected into the hydrothermal synthesis reaction kettle according to the mass percentage of 45%, 17%, 8% and 30%, heated to 130°C, reacted at 1.8MPa for 6h, cooled to room temperature, and took the upper layer The liquid is concentrated and precipitated, and the precipitate is dried at 50°C to obtain a light coupling coagulant solid. The catalyst is dimethyl diallyl ammonium chloride.
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