A kind of naphthalene series ceramic dispersant and preparation method thereof

A ceramic dispersant and naphthalene-based technology, which is applied in the field of ceramic dispersant preparation, can solve the problems of side effects, easy solidification, and narrow degumming range, and achieve good fluidity and viscosity, simple production process, and easy control of conditions.

Active Publication Date: 2018-04-03
黄杏兰
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These dispersants have disadvantages such as narrow dissolving range, easy solidification in a short time, poor adaptability and side effects.
A small number of ceramic enterprises use organic dispersants and inorganic dispersants in combination. Although it can achieve certain effects, the dispersants developed are not universal and cannot be applied to various clay mineral raw materials, so it is difficult to popularize and use them.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A kind of naphthalene series ceramic dispersant and preparation method thereof
  • A kind of naphthalene series ceramic dispersant and preparation method thereof
  • A kind of naphthalene series ceramic dispersant and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0022] A kind of preparation method of naphthalene-based ceramic dispersant of the present invention is made of the following raw material components in proportions by weight:

[0023]

[0024] The acid regulator is any one of amino trimethylene phosphonic acid, ethylenediamine tetramethylene phosphonic acid, hexamethylenediamine tetramethylene phosphonic acid or a mixture of two or more mixed in any ratio;

[0025] The epoxy compound is any one of allyl glycidyl ether, allyl polyoxyethylene epoxy ether and allyl polyoxyethylene polyoxypropylene epoxy ether or two or more are mixed in any ratio mixture;

[0026] The initiator is any one of sodium persulfate, potassium persulfate and ammonium persulfate or a mixture of two or more in any ratio.

[0027] The alkaline conditioner is any one of sodium hydroxide, potassium hydroxide, sodium carbonate and potassium carbonate or a mixture of two or more mixed in any ratio.

[0028] A preparation method of a naphthalene series ce...

Embodiment 1

[0035] A kind of naphthalene-based ceramic dispersant is made from the following raw material components in parts by weight:

[0036]

[0037] Its preparation method is realized through the following steps:

[0038] (1) After adding 2 parts of glucose allylamide, 25 parts of methyl naphthalene sulfonic acid, 2 parts of aminotrimethylene phosphonic acid and 32 parts of water into the reactor, start stirring, and start heating;

[0039] (2) When the temperature rises to 98°C, start to add 10 parts of formaldehyde dropwise for 3 hours;

[0040] (3) add 5 parts of 3-ureapropyl trimethoxysilanes, 2 parts of allyl glycidyl ethers in the reaction kettle again, start to drip the sodium persulfate solution that the mass percent concentration is 5% after waiting to stir evenly, this The sodium persulfate solution is prepared from 1 part of sodium persulfate and 19 parts of water; the dropping time is controlled at 3 hours, and the temperature is controlled at 105°C during the droppi...

Embodiment 2

[0043] A kind of naphthalene-based ceramic dispersant is made from the following raw material components in parts by weight:

[0044]

[0045] Its preparation method is realized through the following steps:

[0046] (1) Add 3 parts of glucose allylamide, 30 parts of methyl naphthalene sulfonic acid, 2 parts of aminotrimethylene phosphonic acid and 22 parts of water into the reactor, start stirring, and start heating;

[0047] (2) When the temperature rises to 105°C, start to add 12 parts of formaldehyde dropwise for 3.5 hours;

[0048] (3) Add 2 parts of 3-ureapropyl trimethoxysilane and 2 parts of allyl polyoxyethylene epoxy ether to the reaction kettle, and start to drop persulfuric acid with a mass percentage concentration of 4% after stirring evenly Sodium solution, the sodium persulfate solution is prepared from 1 part of sodium persulfate and 24 parts of water; the dropping time is controlled at 2 hours, and the temperature is controlled at 110 ° C during the droppin...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention provides a naphthalene-based ceramic dispersant and a preparation method thereof. The steps are as follows: (1) Add glucose allylamide, methylnaphthalenesulfonic acid, acid regulator and water to a reaction kettle, start stirring, and start Heating to raise the temperature; (2) When the temperature rises to 95-120°C, start to add formaldehyde dropwise for 0.5-5 hours; (3) Add 3-ureapropyltrimethoxysilane, cyclic Oxygen compound, after being stirred evenly, start to drop an initiator solution with a mass percent concentration of 1-10%, which is prepared from the initiator and part of the water; the dropping time is controlled at 0.5-4 hours , the temperature is controlled at 90 to 120°C during the dropwise addition; (4) after the dropwise addition, keep the temperature and continue the reaction for 1 to 4 hours, add an alkaline regulator for neutralization, and cool down and discharge the material after the neutralization is completed, to obtain the naphthalene Department of ceramic dispersant.

Description

technical field [0001] The invention belongs to the technical field of preparation of ceramic dispersants, in particular to a naphthalene-based ceramic dispersant and a preparation method thereof. Background technique [0002] Ceramic dispersant, also known as ceramic decoagulant, debonding agent, water reducer and diluent, etc., refers to a surface that can quickly wet the surface of solid particles and raise the energy barrier between solid particles to a high enough level. active agent. The main purpose is to keep the ceramic slurry with good fluidity within a certain period of time, that is, to reduce the surface energy of the particles, to reduce the interfacial tension between solid and liquid, to better and effectively infiltrate small solid particles, and to obtain high solid content and Good fluidity mud. In the preparation of special ceramic slurry, excellent dispersants can not only affect the surface charge of particles, but also change the chemical bond struct...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Patents(China)
IPC IPC(8): C08F220/54C08F216/14C08F8/36C08F8/42C04B35/634
CPCC04B35/63444C08F8/36C08F8/42C08F216/14C08F220/54C08F283/00C08G16/0237C08F2800/20C08F216/1433C08F216/145
Inventor 刘碧霞
Owner 黄杏兰
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap