Production method for in-situ generation of titanium zirconium boride reinforced high-modulus and high-hardness steel
An in-situ generation, boride technology, applied in the field of iron and steel matrix composite materials, can solve the problems of complex process and achieve the effect of inhibiting the iron boron phase
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[0027] A preparation method for in-situ generation of titanium-zirconium boride reinforced high-modulus high-hardness steel, the specific steps are as follows:
[0028] Step 1. First, weigh the boron powder, titanium powder, zirconium powder and high-purity iron powder with a purity of more than 99.99% according to the mass percentage of B3.52%, Ti 7.60%, Zr 5.80%, and put the powder into a ball mill tank Mix the materials with a planetary ball mill, the ball-to-material ratio is 10:1, and the ball milling time is 3 hours;
[0029] Step 2. Take out the mixed powder obtained in step 1, put it in the copper crucible of the vacuum arc melting furnace, and melt it under the protective atmosphere of argon gas, and at the same time, continuously process the melt by electromagnetic stirring to make the melt completely homogenized , while refining the precipitated phase and matrix structure, the sample was cast in a water-cooled copper mold with a cooling rate of 5K s -1 .
[0030] ...
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