Long-acting water-based metal antirust agent and preparation method thereof
A water-based anti-rust agent technology, applied in the coating process of metal materials, etc., can solve problems such as failure of aircraft parts and auto parts, and achieve good lubricity, long acting time, and good environmental protection effects
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Embodiment 1
[0027] The long-acting water-based antirust agent provided in this embodiment is prepared from the following raw materials in parts by weight:
[0028]
[0029] Wherein, the preparation method of the long-chain complex amine borate ester is: 12 mass parts of boric acid, 12 mass parts of triethanolamine, 5 mass parts of tetraethylenepentamine, 3 mass parts of dodecylethyleneamine, 6 mass parts Add 80 parts by mass of polyvinyl alcohol to 80 parts by mass of anhydrous DMSO to obtain a mixed solution, raise the temperature of the mixed solution to 130°C, reflux for 4 hours, distill off DMSO and a small amount of water under reduced pressure, and then add 60 parts by mass of tetrahydrofuran Separating unreacted triethanolamine, tetraethylenepentamine, and dodecylethyleneamine, removing residual tetrahydrofuran, and vacuum drying to obtain a colorless viscous long-chain complex borate ester.
[0030] The preparation method of the above-mentioned long-acting water-based antirust ...
Embodiment 2
[0035] The long-acting water-based antirust agent provided in this embodiment is prepared from the following raw materials in parts by weight:
[0036]
[0037] Wherein, the preparation method of the long-chain compound amine borate ester is: 10 mass parts of boric acid, 12 mass parts of triethanolamine, 7 mass parts of tetraethylenepentamine, 4 mass parts of dodecylethyleneamine, 4 mass parts Add 100 parts by mass of polyvinyl alcohol to 100 parts by mass of anhydrous DMSO to obtain a mixed solution, raise the temperature of the mixed solution to 120°C, reflux for 6 hours, distill off DMSO and a small amount of water under reduced pressure, and then add 50 parts by mass of tetrahydrofuran Separating unreacted triethanolamine, tetraethylenepentamine, and dodecylethyleneamine, removing residual tetrahydrofuran, and vacuum drying to obtain a colorless viscous long-chain complex borate ester.
[0038] The preparation method of the above-mentioned long-acting water-based antiru...
Embodiment 3
[0043]The long-acting water-based antirust agent provided in this embodiment is prepared from the following raw materials in parts by weight:
[0044]
[0045] Wherein, the preparation method of the long-chain complex amine borate ester is: 15 parts by mass of boric acid, 15 parts by mass of triethanolamine, 8 parts by mass of tetraethylenepentamine, 4 parts by mass of dodecylethyleneamine, 8 parts by mass of Add 50 parts by mass of polyvinyl alcohol to 50 parts by mass of anhydrous DMSO to obtain a mixed solution, raise the temperature of the mixed solution to 110°C, reflux for 5 hours, distill off DMSO and a small amount of water under reduced pressure, and then add 80 parts by mass of tetrahydrofuran Separating unreacted triethanolamine, tetraethylenepentamine, and dodecylethyleneamine, removing residual tetrahydrofuran, and vacuum drying to obtain a colorless viscous long-chain complex borate ester.
[0046] The preparation method of the above-mentioned long-acting wate...
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