Spilanthes extract, preparation method thereof and application of spilanthes in skin care product
A technology of golden button flower and extract, applied in the field of golden button flower extract and preparation thereof, can solve the problem of no relevant literature reports and the like, achieve the effects of improving skin pigmentation, avoiding clogging of membrane pore size, and the preparation method being safe and reliable
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[0024] Disclosed in a preferred embodiment of the present invention is a method for preparing the extract of Jasmine Japonica, comprising the following steps:
[0025] S1: dry a part by weight of golden button flowers, add 6a to 10a parts by weight of organic solvent for soaking, and then extract to obtain an extract. After the extract is filtered by suction, it is concentrated under reduced pressure to obtain a part by weight of golden button flower suspension;
[0026] S2: Add 4a to 6a parts by weight of deionized water to a part by weight of the Japonica japonica suspension, centrifuge and pass through filter membranes of at least two pore sizes in sequence to obtain a retentate, concentrate the retentate under reduced pressure, and freeze Dried to obtain the golden button flower powder of b weight part;
[0027] S3: adding b parts by weight of the jelly button flower powder into 4b-6b parts by weight of the dissolving solvent, heating and dissolving to obtain the jellis z...
Embodiment 1
[0037] Embodiment 1: Preparation of golden button flower extract A
[0038]Weigh C buttons by weight, dry, add 8 c parts by weight of 50% by mass ethanol aqueous solution and soak for 40 minutes, then perform dual-frequency ultrasonic extraction, the extraction conditions are 25KHz, 49KHz, the temperature is 20°C, and the extraction time is 20min; After extracting solution is suction-filtered, concentrating under reduced pressure obtains the jellyfish suspension of c weight parts (with raw material weight ratio 1:1); Obtain the jellyfish suspension of equal quality with jellyfish raw material in this step, on the one hand It has ensured that the solvent is removed (that is, if the quality of the jaggery suspension is greater than that of the jaggery raw material, there is still solvent in the jaggery suspension that has not been removed), and on the other hand, it is also prevented from passing through the filter membrane in subsequent steps. Cause clogging membrane pore size ...
Embodiment 2
[0041] Embodiment 2: Preparation of golden button flower extract B
[0042] Weigh the golden button flower of e weight part, dry, add 10e weight part of 60% mass percent acetone aqueous solution and soak for 30min, carry out ultra-high pressure extraction, extraction pressure is 400MPa, time is 2min; Concentration obtains the golden button flower suspension of e weight part (with raw material weight ratio 1:1);
[0043] Add 4e parts by weight of deionized water in e parts by weight of the golden button flower suspension, centrifuge for 10min at a speed of 7500rpm and then pass through the microfiltration membrane with a pore size of 0.45 μm and the ultrafiltration membrane with a molecular weight of 8000KD to collect the ultrafiltration membrane retentate wherein the operating temperature of the microfiltration membrane is 50 DEG C, and the pressure is 0.4MPa; the operating temperature of the ultrafiltration membrane is 50 DEG C, and the pressure is 2MPa; then the ultrafiltrat...
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