Water-based anti-rusting liquid and preparation method thereof

An anti-rust liquid, water-based technology, applied in the direction of metal material coating process, etc., can solve the problems of difficult removal of anti-rust oil, troublesome subsequent procedures, eutrophication of water bodies, etc., to increase the anti-corrosion performance, increase the adsorption strength, The effect of enhancing the wetting ability

Inactive Publication Date: 2016-12-07
TIANCHANG RUNDA METAL ANTIRUST AUX
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Metals are easily corroded by the surrounding environment
People usually choose anti-rust oil for surface treatment of metal, but the anti-rust oil is not easy to remove, which will bring trouble to the subsequent process; water-based anti-rust liquid will not affect the subsequent process, but the early water-based anti-rust liquid contains nitrous acid Salt will cause damage to people and the environment; there are also water-based antirust solutions containing phosphating solutions, which can avoid harm to the human body, but because they contain a large amount of phosphorus, it is easy to cause eutrophication of the water body; at present, some water-based antirust solutions on the market The anti-rust liquid avoids the problem of environmental pollution, but the anti-rust effect is not high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] A water-based antirust liquid, its raw materials include by weight: 20 parts of isopropanolamine, 4 parts of boric acid, 27 parts of dimethyl dodecanoate, 3.5 parts of rare earth corrosion inhibitor, 1.5 parts of sodium molybdate, 5 parts of tartaric acid, 0.2 parts of defoamer, 0.15 parts of surfactant, 0.2 parts of fungicide, 47 parts of water.

[0018] The preparation method of the above-mentioned water-based anti-rust liquid comprises the following steps: weighing the above-mentioned raw materials by weight, mixing boric acid, isopropanolamine, and xylene, refluxing for 9.5 hours, removing xylene by distillation under reduced pressure and reacting to form After adding water, vacuum-dry to obtain material A; mix material A and dimethyl dodecanoate, heat up to 140°C, keep stirring for 6.5h, adjust the temperature to 75°C, and vacuum-dry to obtain material B; After mixing with rare earth corrosion inhibitor, sodium molybdate, tartaric acid, defoamer, surfactant, and fu...

Embodiment 2

[0020] A water-based antirust liquid, its raw materials include by weight: 15 parts of isopropanolamine, 3.1 parts of 200 mesh boric acid, 30 parts of dimethyl dodecanoate, 2 parts of CeCl, 2 parts of sodium molybdate, tartaric acid 4 parts, 0.3 parts of polyoxypropylene glyceryl ether, 0.1 parts of sodium lauryl sulfate, 0.3 parts of isothiazolinone, 42 parts of water.

[0021] The preparation method of the above-mentioned water-based anti-rust liquid comprises the following steps: taking the above-mentioned raw materials by weight, mixing boric acid, isopropanolamine, and xylene, refluxing for 10 hours, and removing the xylene and the reaction product by distillation under reduced pressure. After watering, vacuum-dry to obtain material A, wherein the weight-to-volume (g / ml) ratio of boric acid and xylene is 1:3; mix material A and dimethyl dodecanoate evenly, heat up to 145°C, and keep warm Stir for 6 hours, adjust the temperature to 80°C, and vacuum-dry to obtain material B...

Embodiment 3

[0023] A water-based antirust liquid, its raw materials include by weight: 25 parts of isopropanolamine, 5.2 parts of 150 mesh boric acid, 25 parts of dimethyl dodecanoate, CeNO 3 5 parts, 1 part of sodium molybdate, 6 parts of tartaric acid, 0.1 part of polyoxypropylene polyoxyethylene glyceryl ether, 0.2 part of sodium lauryl sulfate, 0.1 part of isothiazolinone, and 52 parts of water.

[0024] The preparation method of the above-mentioned water-based anti-rust liquid comprises the following steps: weighing the above-mentioned raw materials by weight, mixing boric acid, isopropanolamine, and xylene, refluxing for 9 hours, and removing xylene and the reaction product by distillation under reduced pressure. After watering, vacuum-dry to obtain material A, wherein the weight-to-volume (g / ml) ratio of boric acid and xylene is 1:4; mix material A and dimethyl dodecanoate, heat up to 135°C, and keep warm Stir for 7 hours, adjust the temperature to 70°C, and dry in vacuum to obtai...

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PUM

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Abstract

The invention discloses water-based anti-rusting liquid. The water-based anti-rusting liquid comprises raw materials of, by weight, 15-25 parts of isopropanolamine, 3.1-5.2 parts of boric acid, 25-30 parts of dimethyl dodecanedioate, 2-5 parts of a rare earth corrosion inhibitor, 1-2 parts of sodium molybdate, 4-6 parts of tartaric acid, 0.1-0.3 part of a defoaming agent, 0.1-0.2 part of a surfactant, 0.1-0.3 part of a sterilizing agent and 42-52 parts of water. The invention further discloses a preparation method of the water-based anti-rusting liquid. The preparation method includes the following steps that the raw materials are weighed according to the weight parts, the boric acid, the isopropanolamine and xylene are evenly mixed, and backflow, reduced pressure distillation and vacuum drying are conducted to obtain a material A; the material A and the dimethyl dodecanedioate are evenly mixed, heated and stirred, and then vacuum drying is conducted to obtain a material B; and the material B, the rare earth corrosion inhibitor, the sodium molybdate, the tartaric acid, the defoaming agent, the surfactant and the sterilizing agent are evenly mixed and then stirred after water is added, so that the water-based anti-rusting liquid is obtained. The water-based anti-rusting liquid is good in anti-rusting performance and free of environment pollution.

Description

technical field [0001] The invention relates to the technical field of antirust liquid, in particular to a water-based antirust liquid and a preparation method thereof. Background technique [0002] Metals are easily corroded by the surrounding environment. People usually choose anti-rust oil for surface treatment of metals, but the anti-rust oil is not easy to remove, which will bring trouble to the subsequent process; water-based anti-rust liquid will not affect the subsequent process, but the early water-based anti-rust liquid contains nitrous acid Salt will cause damage to people and the environment; there are also water-based anti-rust solutions containing phosphating solutions, which can avoid harm to the human body, but because they contain a lot of phosphorus, it is easy to cause eutrophication of water bodies; currently, some water-based anti-rust solutions on the market The anti-rust liquid avoids the problem of environmental pollution, but the anti-rust effect is...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C22/40C23F11/08
CPCC23C22/40C23F11/08
Inventor 林伟江海涛江海波江浩
Owner TIANCHANG RUNDA METAL ANTIRUST AUX
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