Preparation method and use method of thermally-sprayed ceramic seal glaze for coal feeding port of coke oven
A technology of ceramic sealing and coal filling port, which is applied in the field of refractory materials, can solve problems such as cracks, time-consuming and labor-intensive problems, and achieve the effects of firm combination, convenient construction, and avoiding coking and carbon deposition
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Embodiment 1
[0021] 1) Preparation of borate composite solvent: formula range: 39 parts of borax, 20 parts of zinc oxide, 19 parts of quartz powder, 8 parts of potash stone, 4.5 parts of cooked talc; mix the ingredients according to the formula for 16 minutes and melt at 1000 °C at high temperature. Then water quenching obtains the complex borate saturated solvent;
[0022] 2) Preparation of thermal spraying glaze: formula range: step 1) 35 parts of composite borate saturated solvent, 25 parts of kaolin, 25 parts of quartz powder, 15 parts of zircon powder, 3.5 parts of calcite, 3.5 parts of talc powder, three 1.1 parts of sodium polyphosphate; after mixing the ingredients according to the proportion, add 45% water of the total mass of the glaze raw materials, and grind for 2 hours to control the particle size to be less than 80% of <10μm, and less than 2% of greater than 50μm to obtain the glaze;
[0023] 3) The pressure spraying method of the spraying machine is adopted, and the pressure...
Embodiment 2
[0027] 1) Preparation of borate composite solvent: formula range: 37 parts of borax, 22 parts of zinc oxide, 17 parts of quartz powder, 8 parts of potassium stone, and 4 parts of cooked talc; mix the ingredients according to the formula for 18 minutes and then melt at 1020 °C at high temperature. Then water quenching obtains the complex borate saturated solvent;
[0028] 2) Preparation of thermal spraying glaze: formula range: 34 parts of composite borate saturated solvent prepared in step 1), 27 parts of kaolin, 24 parts of quartz powder, 16 parts of zircon powder, 3 parts of calcite, 4 parts of talc powder, three 1 part of sodium polyphosphate; after mixing the ingredients according to the proportion, add 55% water of the total mass of the glaze raw materials, and grind for 3.5 hours so that the particle size is controlled at <10μm, more than 80%, and greater than 50μm2% to obtain the glaze;
[0029] 3) The pressure spraying method of the spraying machine is adopted, and the...
Embodiment 3
[0033] 1) Preparation of borate composite solvent: 42 parts of borax, 18 parts of zinc oxide, 21 parts of quartz powder, 7 parts of potassium stone, and 5 parts of cooked talc in the formula range; mix the ingredients according to the formula for 17 minutes and melt at 970 °C for 17 minutes, then Water quenching obtains complex borate saturated solvent;
[0034] 2) Preparation of thermal spraying glaze: formula range: 35 parts of composite borate saturated solvent prepared in step 1), 24 parts of kaolin, 27 parts of quartz powder, 14 parts of zircon powder, 4 parts of calcite, 3 parts of talc powder, three 1.2 parts of sodium polyphosphate; after mixing the ingredients according to the proportion, add 45% water of the total mass of the glaze raw materials, grind for 2.5 hours to control the particle size at <10μm, more than 80%, and greater than 50μm2% to obtain the glaze;
[0035] 3) The pressure spraying method of the spraying machine is adopted, and the pressure is controll...
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