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A kind of sterile ceramic powder slurry for direct molding 3D ceramic printing and its preparation method and application

A ceramic powder, 3D printing technology, applied in the field of 3D printing, can solve the problem of barren ceramic powder not having plasticity, and achieve the effect of simple and reliable control method, direct molding, and high printing accuracy.

Active Publication Date: 2020-04-10
JINGDEZHEN CERAMIC UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, barren ceramic powder itself does not have plasticity, so good additives must be found to make the ceramic slurry directly have good shear thinning performance, so as to realize direct molding of 3D ceramic printing

Method used

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  • A kind of sterile ceramic powder slurry for direct molding 3D ceramic printing and its preparation method and application

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Experimental program
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Effect test

Embodiment 1

[0034] 1. In this embodiment, a method for preparing a sterile ceramic powder slurry for direct molding 3D ceramic printing, the steps are as follows:

[0035] (1) Dissolve 1.1g D-305 in 20.6g deionized water and mix evenly to obtain a dispersant solution;

[0036] (2) 65.0gAl 2 o 3 The powder (d50=0.5μm) is gradually added to the dispersant solution under high-speed stirring (4000rpm) and mixed evenly to obtain suspension A;

[0037] (3) 0.2g of guar gum powder and 0.2g of sodium carboxymethylcellulose powder (viscosity 300-800mPa·s) were also added to suspension A under high-speed stirring conditions to form suspension B;

[0038] (4) Add 2.4g of polyvinyl alcohol and 0.5g of leveling agent MB-26 into the suspension B, and continue stirring for 60 minutes to obtain a sterile ceramic powder slurry for direct molding 3D ceramic printing, with a solid content of 72.2%.

[0039] 2. In this embodiment, an application of sterile ceramic powder slurry for direct molding 3D ceram...

Embodiment 2

[0046] 1. In this embodiment, a method for preparing a sterile ceramic powder slurry for direct molding 3D ceramic printing, the steps are as follows:

[0047] (1) Dissolve 1.1g D-305 in 17.0g deionized water and mix evenly to obtain a dispersant solution;

[0048] (2) 73.1g ZrO 2 The powder (d50=0.8μm) is gradually added to the dispersant solution under high-speed stirring (4000rpm) and mixed evenly to obtain suspension A;

[0049] (3) 0.3g of guar gum powder and 0.2g of sodium carboxymethylcellulose powder (viscosity 300-800mPa·s) were also added to suspension A under high-speed stirring to form suspension B;

[0050] (4) Add 4.2g of polyvinyl alcohol and 0.8g of leveling agent MB-26 into the suspension B, and continue to stir for 60 minutes to obtain a sterile ceramic powder slurry for direct molding 3D ceramic printing with a solid content of 75.6%.

[0051] 2. In this embodiment, an application of sterile ceramic powder slurry for direct molding 3D ceramic printing is u...

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Abstract

The inventiondiscloseslean ceramic powder size for direct-forming 3D ceramic printing. The lean ceramic powder size is prepared from lean ceramic powder, a composite thixotropic agent, a dispersing agent, a thickening agent, a levelling agent and deionized water in a mass ratio being (65-75):(0.2-0.6):(0.9-1.3):(2.0-5.0):(0.5-1.5):(15-30); the lean ceramic powder is one or combination of Al2O3, ZrO2, SiC and Si3N4. The invention further discloses a preparation method and an application of the lean ceramic powder size. The lean ceramic powder size has high solid content and high shear thinning performance, is suitable for preparation of 3D printing ceramic devices with direction forming process and can be gradually dried and cured in a 3D printing process at the room temperature, and accordingly, a set structure is obtained without collapse, the printing precision is high, and the requirement for 3D printing direct-forming can be well met.

Description

technical field [0001] The invention relates to the technical field of 3D printing, in particular to a sterile ceramic powder slurry for direct molding 3D ceramic printing and its preparation method and application. Background technique [0002] 3D printing technology is a technology to manufacture three-dimensional products by adding materials layer by layer through 3D printing equipment based on the designed 3D model. This layer-by-layer accumulation forming technology is also called additive manufacturing. 3D printing integrates digital modeling technology, electromechanical control technology, information technology, material science and chemistry and many other fields. It is a kind of rapid prototyping technology and is known as the core technology of the "third industrial revolution". [0003] 3D printing materials mainly include plastics, metals, resins, rubber, ceramics, etc. Among them, ceramic materials have excellent characteristics such as high strength, high ha...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/10C04B35/48C04B35/622B33Y70/00B33Y10/00
CPCB33Y10/00B33Y70/00C04B35/10C04B35/48C04B35/622C04B2235/6026
Inventor 施德太常启兵邱瀚仡付斌汪永清周健儿
Owner JINGDEZHEN CERAMIC UNIV