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TC21 titanium alloy powder for laser 3D printing and preparation and using methods

A 3D printing, TC21 technology, applied in the direction of metal processing equipment, additive manufacturing, transportation and packaging, etc., can solve the problems of high strength increase the difficulty of forming, titanium alloy is not easy to hot form, high equipment requirements, etc., to achieve low oxygen content, The effect of smooth surface, good fluidity and low defect rate

Active Publication Date: 2017-02-22
NORTHEASTERN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition to the difficulty of hot forming, difficult machining and high cost of titanium alloy itself, TC21 has high strength and increases the difficulty of forming
When traditional methods such as precision casting, precision plastic forming, and powder metallurgy are used to form TC21, there are characteristics such as long cycle time, high equipment requirements, and poor flexibility.

Method used

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  • TC21 titanium alloy powder for laser 3D printing and preparation and using methods
  • TC21 titanium alloy powder for laser 3D printing and preparation and using methods
  • TC21 titanium alloy powder for laser 3D printing and preparation and using methods

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0089] A TC21 titanium alloy powder for laser 3D printing, the composition is by mass percentage: Al: 5.8%, Sn: 1.9%, Zr: 1.8%, Mo: 2.5%, Cr: 1.2%, Nb: 1.9%, Fe: 0.005 %, C: 0.006%, N: 0.009%, H: 0.003%, O: 0.1%, and the balance is Ti.

[0090] The above-mentioned preparation method of TC21 titanium alloy powder for laser 3D printing specifically comprises the following steps:

[0091] Step 1, preprocessing:

[0092] (1) The raw material TC21 titanium alloy is made into a cylinder as an electrode titanium rod. The diameter of the bottom surface of the cylinder is 50mm and the length is 1000mm; then one end of the electrode titanium rod is processed into a 40-degree conical tip with a surface roughness of Ra12 .5. On the other end of the electrode titanium rod, process an annular slot with a width of 8mm and a depth of 4mm, 6mm away from the port of the titanium rod;

[0093] (2) Clean the electrode titanium rod and install it on the electrode control system in the vacuum ind...

Embodiment 2

[0138] A TC21 titanium alloy powder for laser 3D printing, the composition is by mass percentage: Al: 5.9%, Sn: 2.2%, Zr: 2.0%, Mo: 2.6%, Cr: 1.5%, Nb: 1.9%, Fe: 0.006 %, C: 0.006%, N: 0.002%, H: 0.003%, O: 0.08%, and the balance is Ti;

[0139] The above-mentioned preparation method of TC21 titanium alloy powder for laser 3D printing specifically comprises the following steps:

[0140] Step 1, preprocessing:

[0141] (1) The raw material TC21 titanium alloy is made into a cylinder as an electrode titanium rod. The diameter of the bottom surface of the cylinder is 50mm and the length is 1000mm; then one end of the electrode titanium rod is processed into a 40-degree conical tip with a surface roughness of Ra12 .5. On the other end of the electrode titanium rod, process an annular slot with a width of 8mm and a depth of 4mm, 6mm away from the port of the titanium rod;

[0142] (2) Clean the electrode titanium rod and install it on the electrode control system in the vacuum in...

Embodiment 3

[0189] A TC21 titanium alloy powder for laser 3D printing, the composition is by mass percentage: Al: 6.5%, Sn: 2.4%, Zr: 2.2%, Mo: 2.9%, Cr: 1.5%, Nb: 1.9%, Fe: 0.016 %, C: 0.011%, N: 0.005%, H: 0.006%, O: 0.09%, and the balance is Ti.

[0190] The above-mentioned preparation method of TC21 titanium alloy powder for laser 3D printing specifically comprises the following steps:

[0191] Step 1, preprocessing:

[0192] (1) The raw material TC21 titanium alloy is made into a cylinder as an electrode titanium rod. The diameter of the bottom surface of the cylinder is 50mm and the length is 1000mm; then one end of the electrode titanium rod is processed into a 40-degree conical tip with a surface roughness of Ra12 .5. On the other end of the electrode titanium rod, process an annular slot with a width of 8mm and a depth of 4mm, 6mm away from the port of the titanium rod;

[0193] (2) Clean the electrode titanium rod and install it on the electrode control system in the vacuum in...

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Abstract

The invention provides TC21 titanium alloy powder for laser 3D printing and preparation and using methods. The powder is prepared from, by mass, 5.5%-6.7% of Al, 1.7%-2.4% of Sn, 1.7%-2.4% of Zr, 2.4%-3.1% of Mo, 1.0%-1.8% of Cr, 1.8%-2.2% of Nb, 0.004%-0.18% of Fe, 0.004%-0.01% of C, 0.002%-0.009% of N, 0.003%-0.01% of H, 0.08%-0.1% of O and the balance Ti. The preparation method comprises the steps that TC21 titanium alloy is machined into an electrode and then rotates and goes down in a smelting chamber, gas acts on the conical tip of a titanium bar when the tip of the titanium bar is bright white, titanium alloy liquid drops are brought into an atomizing chamber through nozzles to be cooled into alloy powder, and the alloy powder is collected. The using method comprises the steps that after the alloy powder with the particle size ranging from 54 micrometers to 180 micrometers and a substrate are pretreated, the as-deposited TC21 titanium alloy with the good strength and toughness is printed by adopting a laser 3D printer, wherein the tensile strength is 1,100-1,150 Mpa, the yield strength is 1,010-1,030 Mpa, and the elongation rate is 7%-8%.

Description

technical field [0001] The invention belongs to the technical field of high-activity metal powder preparation for laser 3D printing, and in particular relates to a spherical TC21 titanium alloy powder for laser 3D printing and its preparation and use method. [0002] technical background [0003] Titanium and titanium alloys have excellent properties such as low density, high specific strength, and good corrosion resistance, and are widely used in aerospace and other fields. In the past few decades, the alloying theory, comprehensive strengthening and toughening technology and heat treatment process of titanium alloys for aviation have been greatly developed. With the advancement of science and technology and the performance requirements of aircraft, advanced titanium alloy materials are gradually developing towards damage-tolerant titanium alloys with high fracture toughness and low crack growth rate. Foreign developed countries have successfully applied medium-strength Ti-...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C14/00B22F1/00B22F9/08B22F3/105B33Y10/00B33Y70/00
CPCC22C14/00B22F9/082B33Y10/00B33Y70/00B22F2009/0848B22F2009/0896B22F10/00B22F1/05B22F1/065B22F10/34B22F12/50B22F10/50B22F10/32B22F10/28Y02P10/25
Inventor 陈岁元王栋刘常升郭快快魏明炜梁京
Owner NORTHEASTERN UNIV
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