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80results about How to "Smooth particle surface" patented technology

High-nickel ternary positive electrode material with single crystal morphology and preparation method of high-nickel ternary positive electrode material

The invention discloses a high-nickel ternary positive electrode material with single crystal morphology and a preparation method of the high-nickel ternary positive electrode material. The positive electrode material is formed by a base material and a coating layer, wherein the base material is prepared from a high-nickel ternary precursor, a lithium source and a doping agent; the doping agent comprises a doping element, the doping element is a metal element, the coating layer is formed by a coating material, the coating material comprises a coating element, and the coating element is a metalelement and/or a non-metal element. The positive electrode material is obtained by mixing the high-nickel ternary precursor, the lithium source and the doping agent, performing primary sintering, then mixing with the coating material, and performing secondary sintering. The high-nickel ternary positive electrode material disclosed by the invention has the advantages of single crystal morphology,smooth surface, small specific surface area and high compaction density, and the single crystallization of the high-nickel ternary positive electrode material improves the specific capacity and cycleperformance of the positive electrode material and prolongs the service life of the positive electrode material. The preparation method is simple in process, easy to implement and beneficial to industrial large-scale production.
Owner:TIANJIN GUOAN MGL NEW MATERIALS TECH CO LTD

Long-life modified natural graphite cathode material as well as preparation method and use thereof

The invention discloses a long-life modified natural graphite cathode material as well as a preparation method and use thereof. According to the preparation method, natural graphite powder and asphaltare dipped by virtue of a hot isostatic pressure machine, so that holes in graphite particles can be completely filled with asphalt at high temperature and high pressure conditions; and meanwhile, anasphalt coating layer is formed on the surface of the natural graphite powder, and graphitization is carried out so as to obtain the modified natural graphite cathode material with a core-shell structure, wherein synthetic graphite is embedded into the inside and surface of the natural graphite in situ, the filling rate of the synthetic graphite in the holes of the natural graphite is more than or equal to 94%, the surfaces of the particles are smooth, and the spheroidization degrees of the particles are high. According to the preparation method, the primary coulombic efficiency of the modified natural graphite cathode material is more than or equal to 96%, and the capacity retention ratio of the material after being circulated at a room temperature 1C for 1500 cycles is more than or equal to 80%, so that the prepared material is high in primary coulombic efficiency, long in service life and can be used for replacing synthetic graphite for producing powder battery cathode materials, and the cost is greatly lowered. The preparation method is simple in preparation process and low in cost and has relatively high practicability.
Owner:GUANGDONG DONGDAO NEW ENERGY +1

Modified microcrystal graphite cathode material of lithium ion battery as well as preparation method and application thereof

The invention relates to the technical field of lithium ion battery carbon cathode materials and in particular to a modified microcrystal graphite cathode material of a lithium ion battery as well asa preparation method and application thereof. The material has the advantages that (1) a modified core-shell structured natural graphite cathode material with artificial graphite embedded into and onthe surface of natural graphite in situ is prepared, the overall structural properties of natural microcrystal graphite are maintained, pores of the natural microcrystal graphite is filled with the artificial graphite, and the outer surface of the natural microcrystal graphite is wrapped by the artificial graphite; (2) compared with a conventional cathode material, the cathode material prepared byusing the method provided by the invention is good in isotropy, is capable of inhibiting and absorbing expansion of electrodes in the charge and discharge process, is high in primary coulombic efficiency, long in service life and good in high-magnification charge and discharge performance and is capable of replacing artificial graphite to manufacture cathode materials of power batteries, so as tolower the cost greatly; and (3) the method is simple in preparation process, low in cost and relatively high in practicability.
Owner:GUANGDONG DONGDAO NEW ENERGY +1

Preparation method of mechanically fertilized controlled-release fertilizer special for winter wheat

The invention relates to a preparation method of mechanically fertilized controlled-release fertilizer special for winter wheat. The preparation method comprises the following steps: taking urea, monoammonium phosphate, potassium chloride and zinc sulfate according to the proportion, granulating by a high tower to obtain granular core fertilizer; spraying urea solution onto the core fertilizer to form a urea film to obtain urea-coated fertilizer; taking epoxy resin and polyurethane, and adding curing agent T31, diluting agent benzyl glycidyl ether and talcum powder, mixing uniformly to obtain an outer film coating agent; spraying the outer film coating agent onto the urea-coated fertilizer to obtain three double-layer coated controlled-release fertilizer varieties I, II and III with the dosage of the outer film coating agent respectively occupying 3%, 5% and 7% of the urea-coated fertilizer; and further compounding according to the proportion to obtain the controlled-release fertilizer. The preparation method provided by the invention prepares the core fertilizer special for the wheat according to absorption requirements of the winter wheat on nutrition such as nitrogen, phosphorus, potassium and zinc; and then the double-layer coating is adopted, wherein an inner film improves surface characteristics of the fertilizer granules, and an outer film controls the nutrition release, so that controlled-release fertilizer is suitable for the nutrition absorption of the winter wheat and is suitable for mechanical fertilization.
Owner:菏泽金正大生态工程有限公司

Method for using signal molecules for accelerating repair of disintegrated aerobic granular sludge

The invention relates to a method for using signal molecules for accelerating repair of disintegrated aerobic granular sludge. According to the method for using the signal molecules for accelerating repair of the disintegrated aerobic granular sludge, by adding the exogenous AHLs signal molecules to repair the disintegrated the aerobic granular sludge, in a process of repairing structures of the disintegrated aerobic granular sludge, regranulation of the crushed granular sludge is accelerated, after 20-30 days, the disintegrated aerobic granular sludge is basically and completely repaired, therepaired aerobic granular sludge is smooth in particle surface, regular in shape and compact in structure, and has good settling performance, after adding of the exogenous AHLs is stopped, the granular sludge structures are still intact, and the settling performance and the granule density remain at high levels. According to the method for using the signal molecules for accelerating repair of thedisintegrated aerobic granular sludge, by adding the exogenous AHLs temporarily, an excellent repairing effect on the disintegrated aerobic granular sludge is achieved, the repaired granular sludge is intact in structure and good in settling performance, moreover, operation is simple, and practical application is easy.
Owner:SHANDONG UNIV

Preparation method for controlled-release fertilizer special for mechanically applied rice

The invention relates to a preparation method for controlled-release fertilizer special for mechanically applied rice. The preparation method comprises the following steps: performing double-layer coating by using high tower pelleting compound fertilizer as core fertilizer to obtain the corresponding double-layer coating controlled-release fertilizer I, double-layer coating controlled-release fertilizer II and double-layer coating controlled-release fertilizer III, wherein the bottom layer urea coating accounts for 4 to 6 weight percent of the core fertilizer, and the outer layer film coating agent accounts for 2 weight percent, 4 weight percent and 6 weight percent of the urea coated fertilizer respectively based on the total weight of the reclaimed polyethylene film resin and the reclaimed polystyrene foam resin; and mixing the double-layer coating controlled-release fertilizer I, the double-layer coating controlled-release fertilizer II and the double-layer coating controlled-release fertilizer III according to the mass ratio of 1:(1-3):(1-2) to obtain the controlled-release fertilizer special for mechanically applied rice. The controlled-release fertilizer special for mechanically applied rice meets the absorption requirements of the rice on nitrogen, phosphorus and potassium nutrients in the growth stage, is difficult to crush and is suitable for mechanical fertilizer application.
Owner:菏泽金正大生态工程有限公司

Silica with high fluidity and high oil absorption value for washing powder and preparation method thereof

The invention belongs to the technical field of silica preparation, and particularly relates to silica with high fluidity and high oil absorption value for washing powder and a preparation method thereof. The preparation method of silica comprises the following steps: S1, adding water into a reaction kettle, adding a sulfuric acid solution under stirring, performing heating, dropwise adding a sodium silicate solution until a pH value is 3.5-4.5, then simultaneously dropwise adding the sodium silicate solution and the sulfuric acid solution to carry out a cocurrent neutralization reaction, controlling a pH value to be 3.0-5.0, simultaneously stopping addition of the sulfuric acid solution when drop addition of the sodium silicate solution is completed, and further performing stirring; S2, continuously adding the sodium silicate solution, stopping drop addition of the sodium silicate solution when a pH value is 7.0-8.0, and performing maturing; and S3, performing pressure filtration andwashing on the formed silica, and performing spray drying treatment to obtain the silica. The silica has uniform particle size distribution, large specific surface area, high oil absorption value andhigh fluidity, and has good application prospects in washing powder.
Owner:GUANGZHOU FEIXUE MATERIAL TECH

Yacon fruit flake and whole powder multielement joint processing production system

The invention belongs to the technical field of agricultural product processing devices, relates to a pulverizing device, and in particular relates to a yacon fruit flake and whole powder multielementjoint processing production system. A pretreatment unit, a peeling and slicing unit, an anti-browning unit, an anti-caking treatment unit and a high-speed nitrogen flow pulverizing unit are mounted sequentially from the upstream side to the downstream side of the working procedure, wherein the pretreatment unit comprises an airtight decompression tank; an ultrasonic generation device and a magnetic field generation device are arranged in the airtight decompression tank; the peeling unit comprises a centrifugal peeling device and a slicing device; the centrifugal peeling device and the slicingdevice are sequentially mounted; the anti-browning unit comprises an anti-browning induction treatment device, an anti-metal ion induction treatment device and an anti-caramelization browning treatment device; the anti-caking treatment unit comprises a microwave drying device, an anti-caking polarity remover spray device and a freeze drying device; the high-speed nitrogen flow pulverizing unit comprises a nitrogen generating device, a nitrogen tank, a nitrogen pulverizer and a cyclone separator; and the cyclone separator is provided with a multi-stage discharge port.
Owner:SDIC ZHONGLU FRUIT JUICE

Nano TiO2-containing cellulose-based low-temperature phase change energy storage microcapsule and preparation method thereof

The invention discloses a nano TiO2-containing cellulose-based low-temperature phase change energy storage microcapsule and a preparation method thereof; the low-temperature phase change energy storage microcapsule comprises a capsule core and a capsule wall, wherein the capsule core is a core-shell structure composite phase change material formed by wrapping the surface of paraffin with ethylene glycol, and the capsule wall is formed by a carboxymethyl cellulose membrane doped with nano TiO2 particles; the preparation method comprises the steps of firstly, preparing a composite phase change material by using an aqueous phase ethylene glycol solution and oil phase liquid paraffin through a micro-emulsion method; then, preparing the capsule wall by using a carboxymethyl cellulose water solution containing tetrabutyl titanate and a silane coupling agent through a sol-gel reaction to obtain the microcapsule; the microcapsule has average particle size of 3-10 microns, phase-transition temperature of minus 12 to 5 DEG C and an enthalpy value of 170-200J/g; furthermore, the microcapsule also has good heat-conducting property; the microcapsule is simple in preparation technology and easy in large-scale production, and products of the preparation method do not contain inorganic salt and an organic solvent which can easily corrode a container, so that the preparation method is green and environment-friendly.
Owner:CENTRAL SOUTH UNIVERSITY OF FORESTRY AND TECHNOLOGY +1

Lithium-rich manganese-based solid solution positive electrode material for lithium ion battery and preparation method of lithium-rich manganese-based solid solution positive electrode material

The invention discloses a lithium-rich manganese-based solid solution positive electrode material for a lithium ion battery and a preparation method of the lithium-rich manganese-based solid solution positive electrode material. The chemical general formula of the lithium-rich manganese-based solid solution positive electrode material is xLi2MnO3.(1-x)LiNiCoMn<c>O2, wherein x is more than or equal to 0.2 but less than or equal to 0.7, (a+b+c) is equal to 1, a is more than or equal to 0.2 but less than or equal to 0.8, c is more than or equal to 0.1 but less than or equal to 0.5, the lithium-rich manganese-based solid solution positive electrode material is dense in particles, no hollow phenomenon exists, the tap density TD is larger than 2.0g/cm<3>, the particle size distribution coefficient K90 is 0.6-0.9, and K90=(D90-D10)/D50. The lithium-rich manganese-based solid solution positive electrode material has the advantages of good sphericity, dense particles and narrow particle size distribution, the capacity and the electrochemical performance of the lithium-rich manganese-based solid solution positive electrode material can be remarkably improved, and the cycle lifetime of the lithium-rich manganese-based solid solution positive electrode material can be remarkably prolonged; and moreover, according to the preparation method, a complexing agent does not need to use, and the preparation process is simple, is easy and stable to control, is low in production cost, is environmental-friendly, has no pollution and is suitable for industrial production on a large scale.
Owner:BEIJING EASPRING MATERIAL TECH CO LTD

A long-life modified natural graphite negative electrode material and its preparation method and application

The invention discloses a long-life modified natural graphite cathode material as well as a preparation method and use thereof. According to the preparation method, natural graphite powder and asphaltare dipped by virtue of a hot isostatic pressure machine, so that holes in graphite particles can be completely filled with asphalt at high temperature and high pressure conditions; and meanwhile, anasphalt coating layer is formed on the surface of the natural graphite powder, and graphitization is carried out so as to obtain the modified natural graphite cathode material with a core-shell structure, wherein synthetic graphite is embedded into the inside and surface of the natural graphite in situ, the filling rate of the synthetic graphite in the holes of the natural graphite is more than or equal to 94%, the surfaces of the particles are smooth, and the spheroidization degrees of the particles are high. According to the preparation method, the primary coulombic efficiency of the modified natural graphite cathode material is more than or equal to 96%, and the capacity retention ratio of the material after being circulated at a room temperature 1C for 1500 cycles is more than or equal to 80%, so that the prepared material is high in primary coulombic efficiency, long in service life and can be used for replacing synthetic graphite for producing powder battery cathode materials, and the cost is greatly lowered. The preparation method is simple in preparation process and low in cost and has relatively high practicability.
Owner:GUANGDONG DONGDAO NEW ENERGY +1
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