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Sagger used for high-temperature firing and preparation method of sagger

A high-temperature firing and saggar technology, which is applied in the field of high-temperature firing saggar and its preparation, can solve the problems of poor rapid cooling and rapid heat resistance, fast heating and cooling speed, and less thermal shock times of the sagger, and achieve color and Good thermal shock stability, small thermal expansion coefficient, and the effect of improving thermal shock performance

Inactive Publication Date: 2020-02-21
山东莱科陶瓷材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the current saggers have a low service life, poor thermal shock effect, and are prone to cracking at high temperatures, resulting in kiln plugging and high breakage rates.
[0003] The thermal shock performance of the current sagger is not ideal, the main reasons are as follows: First, due to the poor thermal shock effect of alumina itself, Al 2 o 3 The higher the content, the less the number of thermal shocks, and the temperature of firing high-purity alumina materials is generally at the highest temperature of 1000 ° C ~ 1500 ° C, it only takes 6 to 10 hours from room temperature to the highest temperature, and it only takes 3 to 8 hours to keep it warm. 6 to 9 hours, the heating and cooling speed is fast, the current sagger has poor resistance to rapid cooling and rapid heating, and is easy to crack at high temperature
Secondly, in the production of existing saggers, alumina is used as the main raw material to improve the product's shrinkage resistance, thermal shock resistance and temperature resistance, and the bulk density is generally 2.2kg / m 3 left and right, such long-term use of high energy consumption, energy waste
Thirdly, most of the existing saggers are molded by slurry suction. Because the thickness of the product wall and the bottom are different, and the force is different, the composition of the whole product is uneven, there are many weak parts, the crack resistance is poor, and mass production When the product differentiation is large, the quality is unstable

Method used

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  • Sagger used for high-temperature firing and preparation method of sagger

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] This embodiment provides a sagger for high-temperature firing, which is prepared from the following raw materials: 8 parts of binder or 4.5 parts of water reducer, 15 parts of alumina powder, 17.5 parts of white kaolin powder, 17.5 parts of yellow kaolin powder, and 16.5 parts of quartz powder 20.5 parts, 36 mesh white corundum 20.5 parts, 60 mesh white corundum 20.5 parts, 80 mesh white corundum 20.5 parts, 0-1mm white corundum 20.5 parts, 0.5-1 quartz 22.5 parts, 0.2-0.5mm quartz 22.5 parts, 0.1- 0.2mm quartz 20.5 parts, 0-0.5mm fused mullite 15.5 parts, 0.5-1mm fused mullite 15.5 parts and 1-3mm fused mullite 15.5 parts.

[0041] The preparation method comprises the following steps:

[0042] (1) Carry out magnetic separation to all raw materials, check the impurity iron, and use it after the iron content reaches the standard;

[0043] (2) Mix the alumina powder, kaolin powder, clay powder, white corundum, quartz, mullite, water reducer and water magnetically separat...

Embodiment 2

[0048] The difference between this example and Example 1 is: 1 part of binder, 5 parts of alumina powder, 30 parts of white kaolin powder, 5 parts of yellow kaolin powder, 30 parts of quartz powder, 1 part of 36 mesh white corundum, 60 mesh 40 parts of white corundum, 40 parts of 80 mesh white corundum, 1 part of 0-1mm white corundum, 40 parts of 0.5-1 quartz, 5 parts of 0.2-0.5mm quartz, 40 parts of 0.1-0.2mm quartz, 0-0.5mm 1 part of fused mullite, 30 parts of fused mullite of 0.5-1 mm and 1 part of fused mullite of 1-3 mm.

Embodiment 3

[0050] The difference between this example and Example 1 is: 8 parts of water reducer, 25 parts of alumina powder, 5 parts of white kaolin powder, 30 parts of yellow kaolin powder, 3 parts of quartz powder, 40 parts of 36 mesh white corundum, 60 1 part of white corundum, 1 part of 80 mesh white corundum, 40 parts of 0-1mm white corundum, 5 parts of 0.5-1mm quartz, 40 parts of 0.2-0.5mm quartz, 1 part of 0.1-0.2mm quartz, 0-0.5mm 30 parts of fused mullite, 1 part of fused mullite of 0.5-1mm and 30 parts of fused mullite of 1-3mm.

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Abstract

The invention relates to a sagger used for high-temperature firing and a preparation method of the sagger. The sagger used for high-temperature firing is formed by performing mixing forming by using aluminum oxide powder, kaolin powder, clay powder, white corundum, quartz and mullite as raw materials and performing high-temperature firing. The sagger used for high-temperature firing provided by the invention has a good thermal shock effect, low costs and long service life, and can maintain the crack resistance, uniformity and quality stability of a product during mass production, and is suitable for use in environments with larger temperature differences; the sagger used for high-temperature firing provided by the invention is produced during high-temperature firing, and compared with a sagger formed by synthesizing quartz and mullite in advance and performing mixing forming on the market, the sagger provided by the invention has a more uniform finished-product phase, better color andthermal shock stability, and a small phase thermal expansion coefficient, thereby having extremely high thermal shock stability; and the quartz is added, so that the thermal shock performance can be improved.

Description

technical field [0001] The invention relates to a sagger for high-temperature firing, in particular to a sagger for high-temperature firing and a preparation method thereof. Background technique [0002] The sagger is mainly used for high-temperature sintering (1000°C-1500°C) of high-purity alumina materials when high-purity alumina is fired at high temperature. The main component of the current sagger is Al 2 o 3 Mainly mullite or high alumina material. However, the current saggers have low service life, poor thermal shock effect, and are prone to cracking at high temperatures, resulting in kiln plugging and high breakage rates. [0003] The thermal shock performance of the current sagger is not ideal, the main reasons are as follows: First, due to the poor thermal shock effect of alumina itself, Al 2 o 3 The higher the content, the less the number of thermal shocks, and the temperature of firing high-purity alumina materials is generally at the highest temperature of ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/18C04B35/622C04B35/626
CPCC04B35/18C04B35/622C04B35/62605C04B2235/349C04B2235/6023C04B2235/77C04B2235/96C04B2235/9607
Inventor 王哲
Owner 山东莱科陶瓷材料有限公司
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