Composite ceramic material with high specific surface area and preparation method of composite ceramic material
A high specific surface area, composite ceramic technology, applied in the field of composite materials, can solve the problems of cumbersome preparation process, high energy consumption, low strength, etc., and achieve the effect of high specific surface area, strong adsorption capacity and developed mesopores
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Embodiment 1
[0015] A high specific surface area composite ceramic material, in parts by weight, the raw materials are: 4 parts of carbon fiber, 20 parts of ceramic particles, 2 parts of polyvinyl isobutyl ether, 0.5 parts of alumina powder, 2 parts of silicon carbide powder, magnesium oxide powder 2 servings.
[0016] A preparation method of a high specific surface area composite ceramic material, the specific steps are:
[0017] (1) First, mix the ceramic particles, alumina powder, silicon carbide powder and magnesium oxide powder, then put them into the reaction kettle, carry out the melting reaction under 10MPa pressure and nitrogen protection, and obtain the mixture after cooling;
[0018] (2) Then, mix the mixture with carbon fiber and polyvinyl isobutyl ether, and use ultrasonic oscillation treatment under anhydrous conditions. The power of ultrasonic oscillation treatment is 400W, the time is 4.5h, and it is dried at 4°C to obtain High specific surface area composite ceramic mater...
Embodiment 2
[0021] A high specific surface area composite ceramic material, in parts by weight, the raw materials are: 5 parts of carbon fiber, 23 parts of ceramic particles, 2 parts of polyvinyl isobutyl ether, 0.7 parts of alumina powder, 2 parts of silicon carbide powder, alumina magnesium 2 parts of powder.
[0022] A preparation method of a high specific surface area composite ceramic material, the specific steps are:
[0023] (1) First, mix the ceramic particles, alumina powder, silicon carbide powder and magnesium oxide powder, then put them into the reaction kettle, carry out the melting reaction under 10MPa pressure and nitrogen protection, and obtain the mixture after cooling;
[0024] (2) Then, mix the mixture with carbon fiber and polyvinyl isobutyl ether, and use ultrasonic oscillation treatment under anhydrous conditions. The power of ultrasonic oscillation treatment is 400W, the time is 4.5h, and it is dried at 4°C to obtain High specific surface area composite ceramic mat...
Embodiment 3
[0027] A high specific surface area composite ceramic material, in parts by weight, the raw materials are: 7 parts of carbon fiber, 25 parts of ceramic particles, 3 parts of polyvinyl isobutyl ether, 0.9 parts of alumina powder, 3 parts of silicon carbide powder, magnesium oxide powder 4 parts.
[0028] A preparation method of a high specific surface area composite ceramic material, the specific steps are:
[0029] (1) First, mix the ceramic particles, alumina powder, silicon carbide powder and magnesium oxide powder, then put them into the reaction kettle, carry out the melting reaction under 10MPa pressure and nitrogen protection, and obtain the mixture after cooling;
[0030] (2) Then, mix the mixture with carbon fiber and polyvinyl isobutyl ether, and use ultrasonic oscillation treatment under anhydrous conditions. The power of ultrasonic oscillation treatment is 400W, the time is 4.5h, and it is dried at 4°C to obtain High specific surface area composite ceramic material...
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