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Preparation method of environment-friendly high-efficient compound soaping agent

A complex soap, high-efficiency technology, applied in the direction of detergent compounding agents, chemical instruments and methods, detergent compositions, etc., can solve the problems of unsatisfactory soaping effect, stains, and many foams, and achieve remarkable soaping effect, High cleaning efficiency and the effect of improving the color fastness of fabrics

Inactive Publication Date: 2017-03-22
CHANGZHOU YAHUAN ENVIRONMENTAL PROTECTION TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The technical problem mainly solved by the present invention: aiming at the unsatisfactory soaping effect of the current soaping agent, severe discoloration, need to be heated for use, and there are many foams during washing, need to consume a large amount of water for washing, and may also cause stains. The preparation method of the environment-friendly and high-efficiency composite soaping agent, the method extracts the enzymes and beneficial substances in bitter gourd, duck liver and corn silk through yeast fermentation, purifies by centrifugation, activated carbon decolorization, etc., and prepares the base liquid of the environment-friendly and high-efficiency composite soaping agent, and then Illite is used as the base material, calcined at high temperature, then mixed with dodecyl mercaptan and other substances for modification, and then mixed with environmental protection and high-efficiency composite soaping agent base liquid, maleic anhydride, etc., and the modified illite is free Release negative ions and far infrared to improve enzyme activity, improve soaping effect, suppress foam generation, and finally cool down to obtain environmentally friendly and efficient compound soaping agent. color, improve the color fastness of fabrics, and the soaping agent does not need heating when used, no foam when cleaning, high cleaning efficiency, and will not pollute the environment at the same time, has a broad application market

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0019]First, according to the mass ratio of 3:2:1, take balsam pear, duck liver and corn silk and put them into a masher, and mash them at 1000r / min for 10min. In parts by weight, take 35 parts of mashed mixture, 13 parts of distilled water, Put 10 parts of yeast extract, 7 parts of peptone, 1 part of ammonium chloride and 0.6 part of sodium oxalate into the fermenter, then add the crushed mixture of 1.3% dry yeast, set the temperature at 28°C, and stir and ferment at 120rpm for 2 days; After the above-mentioned fermentation is completed, mix the fermentation mixture and the mixed solution in the fermenter evenly at a mass ratio of 1:2, and place them in an ultrasonic oscillator for ultrasonic oscillation for 10 minutes, and after standing for 10 hours, carry out vacuum filtration, collect the filtrate and put it in In the high-pressure homogenizer, the set temperature is 15°C, the pressure is 60MPa, the set working time is 5min, and the slurry is collected. The mixed solution ...

example 2

[0022] First, according to the mass ratio of 3:2:1, take balsam pear, duck liver and corn silk and put them into a masher, and mash them at 1000r / min for 13min, and take 38 parts of mashed mixture, 15 parts of distilled water, Put 13 parts of yeast extract, 8 parts of peptone, 1.5 parts of ammonium chloride and 0.8 parts of sodium oxalate into the fermentation tank, then add 1.5% dry yeast into the crushed mixture, set the temperature at 34°C, and stir and ferment at 120rpm for 3 days; After the above-mentioned fermentation is completed, mix the fermentation mixture and the mixed solution in the fermenter evenly at a mass ratio of 1:2, and place them in an ultrasonic oscillator for 13 minutes of ultrasonic oscillation, and after standing still for 13 hours, carry out vacuum filtration, collect the filtrate and put it in In the high-pressure homogenizer, the set temperature is 18°C, the pressure is 63MPa, the set working time is 6min, and the slurry is collected. The mixed solut...

example 3

[0025] First, according to the mass ratio of 3:2:1, take balsam pear, duck liver and corn silk and put them into a masher, and mash them at 1000r / min for 15min. In parts by weight, take 40 parts of mashed mixture, 16 parts of distilled water, Put 15 parts of yeast extract, 9 parts of peptone, 2 parts of ammonium chloride and 0.9 part of sodium oxalate into the fermenter, then add the crushed mixture of 1.6% dry yeast, set the temperature at 36°C, stir and ferment at 120rpm for 4 days; After the above-mentioned fermentation is finished, the fermentation mixture in the fermenter and the mixed solution are mixed evenly at a mass ratio of 1:2, and placed in an ultrasonic oscillator for ultrasonic oscillation for 15 minutes, and then left to stand for 15 hours before being filtered under reduced pressure, and the filtrate is collected and put into In the high-pressure homogenizer, the set temperature is 20°C, the pressure is 65MPa, the set working time is 7min, and the slurry is col...

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PUM

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Abstract

The invention discloses a preparation method of an environment-friendly high-efficient compound soaping agent. The preparation method of the environment-friendly high-efficient compound soaping agent belongs to the technical field of soaping agent preparation, and comprises the steps of extracting enzymes and beneficial substances in bitter gourds, duck livers and corn stigmas through yeast fermentation; preparing an environment-friendly high-efficient compound soaping agent base solution through purifying by centrifuging, actived carbon decoloring and the like; adopting illite as a base stock, calcining at high temperature, mixing with substances such as lauryl mercaptan so as to be modified, then mixing with the environment-friendly high-efficient compound soaping agent base solution, maleic anhydride and the like, and freely releasing anion and far infrared through the modified illite, so that the enzymatic activity is improved, the soaping effect is improved, and the foam generation is inhibited; finally, cooling to obtain the environment-friendly high-efficient compound soaping agent. The soaping agent prepared by the invention has a remarkable soaping effect, can be used for effectively removing fabric surface dyeing and improving fabric color fastness, has no need to be heated when in use, has no foam during washing, is high in cleaning efficiency, cannot pollute the environment at the same time, and has wide application market.

Description

technical field [0001] The invention discloses a preparation method of an environment-friendly and high-efficiency composite soaping agent, and belongs to the technical field of soaping agent preparation. Background technique [0002] The soaping process after textile dyeing and printing can remove the floating color on the surface of the fabric and improve the fastness of the dyed fabric. Adding soaping agent can improve the effect of washing and removing floating color, and make the dye no longer stick to the fabric through dispersion, suspension and complexation, so as to achieve the purpose of improving soaping fastness and anti-staining. With the increasing demand for high-grade composite fiber fabrics, the demand for soaping agents is also increasing. [0003] Soaping agent is a post-processing auxiliary commonly used in printing and dyeing factories. It mainly plays the role of washing away reactive dyes that are not firmly combined with fibers and removing printing ...

Claims

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Application Information

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IPC IPC(8): C11D7/60C11D7/42C11D7/02C11D7/26C11D7/34C11D7/10
CPCC11D3/386C11D7/02C11D7/10C11D7/26C11D7/34C11D7/40C11D7/44C11D7/46
Inventor 高玉梅邹玉薛蕾
Owner CHANGZHOU YAHUAN ENVIRONMENTAL PROTECTION TECH