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A processing device and method for a flowback fracturing fluid

A technology of fracturing flowback fluid and treatment equipment, which is applied in chemical instruments and methods, multi-stage water/sewage treatment, water/sludge/sewage treatment, etc., and can solve complex components, poor treatment effect, and large floor area and other problems, to achieve the effect of simple process flow, flexible and convenient use, and small footprint

Active Publication Date: 2017-04-19
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] However, the fracturing fluid has high viscosity, complex composition, and difficult treatment. The existing treatment methods all have the disadvantages of large consumption of chemicals, complicated process, high treatment cost, and large floor area. Therefore, it is necessary to develop a method for the treatment and reuse of fracturing flowback fluid with good treatment effect, low cost and small footprint

Method used

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  • A processing device and method for a flowback fracturing fluid
  • A processing device and method for a flowback fracturing fluid

Examples

Experimental program
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Effect test

Embodiment 1

[0075] This embodiment is used to illustrate the method for treating fracturing flowback fluid using the device for treating fracturing flowback fluid of the present invention.

[0076] (1) Under the condition that the pH value of the fracturing flowback fluid is 3, the oxidation viscosity reduction reaction is carried out in the oxidation viscosity reduction reaction chamber 1 in the presence of an oxidizing agent and a catalyst. The oxidizing agent is 10% by weight of sodium persulfate solution, and the catalyst is It is a mixture of ferric chloride and calcium chloride, the weight ratio of ferric chloride and calcium chloride is 1:4, and the dosage of oxidant is 200ppm relative to the inflow of fracturing flowback fluid (based on the effective sodium persulfate concentration meter), the dosage of catalyst is 200ppm, and the hydraulic retention time in oxidation viscosity reduction reaction chamber 1 is 30min;

[0077] (2) The material after the step (1) reaction enters the ...

Embodiment 2

[0081] This embodiment is used to illustrate the method for treating fracturing flowback fluid using the device for treating fracturing flowback fluid of the present invention.

[0082] (1) Under the condition that the pH value of the fracturing flowback fluid is 4, the oxidation viscosity reduction reaction is carried out in the oxidation viscosity reduction reaction chamber 1 in the presence of an oxidizing agent and a catalyst. The oxidizing agent is 15% by weight of sodium persulfate solution, and the catalyst is It is a mixture of ferric chloride and calcium chloride, the weight ratio of ferric chloride and calcium chloride is 1:6, relative to the fracturing flowback fluid, the dosage of oxidant is 100ppm (based on the effective sodium persulfate concentration meter), the dosage of catalyst is 500ppm, and the hydraulic retention time in oxidation viscosity reduction reaction chamber 1 is 15min;

[0083] (2) The material after the step (1) reaction enters the mixing zone 2...

Embodiment 3

[0087] This embodiment is used to illustrate the method for treating fracturing flowback fluid using the device for treating fracturing flowback fluid of the present invention.

[0088] (1) Under the condition that the pH value of the fracturing flowback fluid is 5, the oxidation viscosity reduction reaction is carried out in the oxidation viscosity reduction reaction chamber 1 in the presence of an oxidizing agent and a catalyst. The oxidizing agent is 20% by weight of sodium persulfate solution, and the catalyst is It is a mixture of ferric chloride and calcium chloride, the weight ratio of ferric chloride and calcium chloride is 1:8, and the dosage of oxidant is 300ppm relative to the inflow of fracturing flowback fluid (based on the effective rate of sodium persulfate concentration meter), the dosage of catalyst is 350ppm, and the hydraulic retention time in oxidation viscosity reduction reaction chamber 1 is 45min;

[0089] (2) The material after the step (1) reaction ent...

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Abstract

The invention relates to the technical field of oilfield fracturing, and discloses a processing device for a flowback fracturing fluid. The device includes an oxidation viscosity-reducing reaction chamber, an oil-removing turbidity-reducing reaction chamber and a separating and settling chamber. The oxidation viscosity-reducing reaction chamber is in the oil-removing turbidity-reducing reaction chamber. The oil-removing turbidity-reducing reaction chamber is in the separating and settling chamber. The oxidation viscosity-reducing reaction chamber is communicated with a feeding apparatus. The oil-removing turbidity-reducing reaction chamber includes a mixing zone, a flocculation zone, a filtration zone and a clear water zone from bottom to top. An alkali liquid feeding pipe is in the mixing zone. The cross section of the flocculation zone is an inverted trapezoid. A waste dreg collecting barrel is disposed in the filtration zone and is communicated with the separating and settling chamber through an overflow pipe. The clear water zone is provided with a first water discharging pipe. The upper part of the separating and settling chamber is provided with a second water discharging pipe, and the lower part of separating and settling chamber is provided with a dreg discharging pipe. A processing method of the flowback fracturing fluid is also disclosed. The device is low in occupied space. The device and the method are low in processing cost and good in processing effects, and can be widely applied for processing and recycle of oilfield flowback fracturing fluids.

Description

technical field [0001] The invention relates to a waste water treatment device and method, in particular to a treatment device and method that can be reused after oil field fracturing flowback fluid is treated. Background technique [0002] With the development of the world economy, the demand for energy in countries around the world continues to increase, while the conventional oil and gas resources are increasingly depleted. new growth point. [0003] The development of unconventional oil and gas resources such as shale gas usually requires the use of multi-stage staged fracturing technology for large horizontal wells, thus requiring the use of a large amount of fracturing fluid. [0004] Due to the large amount of fluid used and flowback in the fracturing development process of the existing unconventional oil and gas resources, a large amount of fracturing waste fluid is produced, with complex components, high suspended solids and oil content. Fluctuating water quality,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F9/04
Inventor 高峰曹晓磊
Owner CHINA PETROLEUM & CHEM CORP
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