Efficient synthetic method for series of spinel nanostructured materials

A technology of nanostructures and synthesis methods, applied in chemical instruments and methods, metal/metal oxide/metal hydroxide catalysts, physical/chemical process catalysts, etc., can solve complex steps, high cost, unsuitable for mass production and other problems, to achieve the effect of simple reaction device, realization of industrial scale production, and simple synthesis steps

Active Publication Date: 2017-04-26
XIAMEN UNIV +1
View PDF2 Cites 9 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These methods have their own advantages and disadvantages. The prominent problems are high cost and complicated steps. They are only suitable for a small amount of synthesis in the laboratory and are not suitable for mass production.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Efficient synthetic method for series of spinel nanostructured materials
  • Efficient synthetic method for series of spinel nanostructured materials
  • Efficient synthetic method for series of spinel nanostructured materials

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0020] Embodiments of the present invention include the following steps:

[0021] 1) Dissolving the soluble salt of A and the soluble salt of B in an alcoholic solvent and stirring to obtain a mixed solution; the A is selected from one of Mg, Zn, Ni, Co, Ca, Cu, rare earth element Ln, etc. ; The B is selected from one of Al, Si, Cr, Bi, Fe, Ga, etc.; the soluble salt adopts nitrate or chloride etc.; the mol ratio of the soluble salt of A and the soluble salt of B can be The ratio is 1:2; the alcohol solvent can be selected from at least one of ethanol, propanol, butanol, hexanol, etc.; the stirring time can be 1 h.

[0022] 2) Transfer the mixed solution obtained in step 1) to an autoclave for reaction, and centrifuge to obtain a precursor product; the autoclave can be an autoclave lined with polytetrafluoroethylene; the temperature of the reaction can be 200 °C, the reaction time can be 24h.

[0023] 3) Calcining the precursor product obtained in step 2) to obtain a series ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention provides an efficient synthetic method for a series of spinel nanostructured materials and relates to nanostructured materials. The efficient synthetic method comprises the steps that soluble salts of A and B are dissolved in an alcohol solvent and stirred, and a mixed solution is obtained, wherein A is one of Mg, Zn, Ni, Co, Ca and Cu, B is one of Al, Si, Cr, Bi, Fe and Ga, and the soluble salts adopt nitrates or chlorides; the mixed solution is transferred into an autoclave for a reaction, a precursor is obtained through centrifugation, and the series of spinel nanostructured materials can be obtained after calcination. The method has remarkable advantages in low-cost massive synthesis, and is wide in application range and suitable for synthesizing different kinds and morphologies of spinel and spinel-like nanomaterials, and product purity is high. Cheap and safe raw materials and simple synthesis steps are adopted, a reaction device is simple, and a reaction solvent can be recycled.

Description

technical field [0001] The invention relates to nanostructure materials, in particular to an efficient synthesis method of a series of spinel nanostructure materials. Background technique [0002] In recent years, spinel (AB 2 o 4 ) materials have attracted widespread attention in both academia and industry because of their excellent physical and chemical properties, including high melting point, high hardness, high mechanical strength, low thermal expansion coefficient, good thermal shock resistance, and chemical inertness. At present, spinel materials are widely used in refractory materials, high temperature infrared windows, humidity sensors, catalysis and so on. Spinel is a widely used functional material, but there are very few naturally occurring spinels, so it needs to be synthesized artificially to meet various application requirements. [0003] The most common method for artificially synthesizing spinel materials is to generate spinel materials in one step throug...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): B01J23/00B01J37/08B01J37/10B01J35/10
CPCB01J23/005B01J35/1004B01J37/08B01J37/10
Inventor 张先华王理杨海亮刘畅林敬东王勇
Owner XIAMEN UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap