Low-temperature cold sintering preparation method of barium titanate ferroelectric ceramic
A technology of ferroelectric ceramics and barium titanate, which is applied in the field of sintering and preparation of barium titanate ferroelectric ceramics, can solve the problems of uncontrollable key performance indicators, restrict mass production, increase in grain size, etc., and achieve broad industrial application Prospects, effects of excellent dielectric properties and impact toughness, low energy consumption
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Embodiment 1
[0020] Ba(OH) 2 and TiO 2 The powder is put into the solvent (the solvent is deionized water) according to the molar ratio of 1.2:1, ultrasonically dispersed and stirred for 20-40min to prepare a suspension with a Ba(OH)2 concentration of 0.1mol / L.
[0021] Select BaTiO with a purity of 99.5% and an average particle size of 40 nm 3 Nanoscale powder and BaTiO with a purity of 99.9% and an average particle size of 400nm 3 Submicron powder, according to the size of the prepared BaTiO3 ceramics and related devices, calculate the quality of the required BaTiO3 powder, add BaTiO3 nanometer powder and BaTiO3 submicron powder according to the mass ratio of 1:1, add 25wt.% in step 1 The prepared Ba(OH)2 / TiO2 suspension was ground in a mortar for 0.5-1 h.
[0022] After cold pressing at room temperature for 10 minutes, keep the temperature at 180°C and hold the pressure for 3 hours, and the pressure is 450MPa. BaTiO 3 The ceramic preform was dried at 200° C. for 12 hours.
[0023]...
Embodiment 2
[0026] Ba(OH) 2 and TiO 2The powder is put into the solvent (the solvent is deionized water) according to the molar ratio of 1.2:1, ultrasonically dispersed and stirred for 30min to obtain Ba(OH) 2 A suspension with a concentration of 0.1mol / L.
[0027] Select BaTiO with a purity of 99.8% and an average particle size of 50nm 3 Nanoscale powder and BaTiO with a purity of 99.9% and an average particle size of 500nm 3 Submicron powder. According to preparing BaTiO3 pottery and related device size, calculate the required BaTiO3 powder quality, with BaTiO3 nanoscale powder and BaTiO3 submicron powder according to the ratio of mass ratio 1:1, add the prepared Ba in 25wt.% step 1 ( OH)2 / TiO2 suspension was ground in a mortar for 0.5-1h.
[0028] After cold pressing at room temperature for 15 minutes, keep the temperature at 200°C and keep the pressure for 3 hours, the pressure is 500MPa. BaTiO 3 The ceramic preform was dried at 200°C for 18 hours.
[0029] Carry out vacuum pr...
Embodiment 3
[0032] Ba(OH) 2 and TiO 2 The powder is put into the solvent (the solvent is deionized water) according to the molar ratio of 1.2:1, ultrasonically dispersed and stirred for 40min to obtain Ba(OH) 2 A suspension with a concentration of 0.1mol / L.
[0033] Select BaTiO with a purity of 99.99% and an average particle size of 40nm 3 Nanoscale powder and BaTiO with a purity of 99.9% and an average particle size of 500nm 3 Submicron powder. According to preparing BaTiO3 pottery and related device size, calculate the required BaTiO3 powder quality, with BaTiO3 nanoscale powder and BaTiO3 submicron powder according to the ratio of mass ratio 1:1, add the prepared Ba in 25wt.% step 1 ( OH)2 / TiO2 suspension was ground in a mortar for 0.5-1h.
[0034] After cold pressing at room temperature for 20 minutes, keep the temperature at 200°C and hold the pressure for 3 hours, the pressure is 450MPa. BaTiO 3 The ceramic preform was dried at 200° C. for 12 hours.
[0035] Carry out press...
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