A kind of synthetic supercharged methanol engine oil and its preparation method and application
A methanol engine, synthetic base oil technology, applied in the petroleum industry, lubricating compositions, base materials, etc., can solve the problems of synthetic supercharged engine wear, strong water absorption, engine failure, etc.
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Embodiment 1
[0037] Put 97 parts by mass of synthetic base oil A (1-hexene, 1-octene and 1-dodecene in a 1:4:5 molar ratio in a high-pressure reactor with a vacuum, sample delivery and stirring device After evacuating, let in nitrogen and add the catalyst triisobutylaluminum and dicyclopentadienyl zirconium dichloride in a mass ratio of 3:1. The total mass of the catalyst is 1-hexene, 1-octene, and 1-decene. 1% of the total mass of diene, keep the reactor at 20℃ to react for 2h, after the reaction is uniformly removed insolubles, it is prepared, the 100℃ kinematic viscosity of the obtained synthetic base oil A is 60.4mm 2 / s) Put it into a three-necked flask with a stirring device and a water bath. The water bath is kept at a constant temperature of 60°C, and then 1 part by mass of N-phenyl-2-naphthylamine and 1 part by mass of primary zinc dialkyl dithiophosphate are added. , 0.3 parts by mass of benzotriazole, 0.3 parts by mass of high-base calcium sulfonate, 0.3 parts by mass of polymeriz...
Embodiment 2
[0039] Put 96.5 parts by mass of synthetic base oil A (1-hexene, 1-octene and 1-dodecene in a high-pressure reactor with a vacuum, sample delivery and stirring device in a molar ratio of 1.5:4:4.5 After evacuating for several times, let in nitrogen gas, add the catalyst triisobutylaluminum and dicyclopentadienyl zirconium dichloride in a mass ratio of 3:1. The total mass of the catalyst is 1-hexene, 1-octene, 1 -1.5% of the total mass of dodecene. Keep the reactor at 20℃ for 2h. It is prepared after the insoluble matter is removed evenly. The kinematic viscosity of synthetic base oil A at 100℃ is 82.7mm. 2 / s) was added to a three-necked flask with a stirring device and a water bath, the water bath was kept at a constant temperature of 60°C, and then 1 part by mass of 4,4'-dioctyldiphenylamine, 1 part by mass of disulfide phosphate, and 0.5 part by mass of primary Zinc alcohol dialkyl dithiophosphate, 0.3 parts by mass tolyltriazole, 0.3 parts by mass of calcium high base alkyl ...
Embodiment 3
[0041] Put 97 parts by mass of synthetic base oil B (1-hexene, 1-octene and 1-dodecene according to the molar ratio of 0.5:5.5:4 in a high-pressure reactor with vacuum, sample delivery and stirring devices After evacuating for several times, let in nitrogen gas, add the catalyst triisobutylaluminum and dicyclopentadienyl zirconium dichloride in a mass ratio of 2:1. The total mass of the catalyst is 1-hexene, 1-octene, 1 -1% of the total mass of dodecene, keep the reactor at 20℃ to react for 2h, after the reaction is uniformly removed insolubles, it is prepared, the 100℃ kinematic viscosity of the obtained synthetic base oil B is 101.3mm 2 / s) Put it into a three-necked flask with a stirring device and a water bath. The water bath is kept at a constant temperature of 60°C, and then 1 part by mass of diisooctyl diphenylamine, 1 part by mass of primary alcohol zinc dialkyl dithiophosphate, 0.3 mass Parts of thiadiazole derivatives, 0.3 parts by mass of calcium sulfonate of high bas...
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