A kind of hard pure gold sealing material and preparation method thereof
A kind of filling and hard technology, which is applied in the field of hard gold filling materials and its preparation, can solve the problems of high melting temperature, difficulty in popularization, and difficulty in wide-scale promotion, so as to achieve grain refinement and improve comprehensive mechanical properties. performance effect
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Embodiment 1
[0025] Firstly prepare the filling material, and carry out batching according to the weight ratio, dysprosium 75.0%, indium 13.2%, zinc 3.5%, cobalt powder 8.3%, the average diameter of cobalt powder is 2mm. Two metals, dysprosium and indium, are placed in a graphite crucible, and zinc block and cobalt powder are placed in two compartments in the interlayer on the furnace top, and the interlayer can be poured and fed by external mechanical control. Vacuum to 5*10 after closing the furnace door -3 Pa, and then filled with argon, the pressure is 0.8 atmospheres. Under the protection of an inert atmosphere, the dysprosium-indium binary alloy was smelted in proportion. The melting temperature reached 1450°C to completely melt the binary alloy, and then the power was lowered to reduce the melt temperature to 1150°C. Zinc block and cobalt powder were added in sequence quickly, and the The crucible is vibrated and stirred, and cast into a pre-placed mold to obtain pure gold filling ...
Embodiment 2
[0029] First of all, the filling material is prepared, and the ingredients are prepared according to the weight ratio, dysprosium 80.0%, indium 14.1%, zinc block 2.0%, cobalt powder 3.9%, and the average diameter of the cobalt powder is 1mm. Two metals, dysprosium and indium, are placed in a graphite crucible, and zinc block and cobalt powder are placed in the interlayer of the furnace top in two compartments. Vacuum to 3*10 after closing the furnace door -3 Pa, and then filled with argon, the pressure is 0.8 atmospheres. Under the protection of an inert atmosphere, the dysprosium-indium binary alloy is melted in proportion, and the melting temperature reaches 1400°C to completely melt the binary alloy, and then the power is reduced to 1200°C, and the zinc block and cobalt powder are quickly added in turn, and the crucible Vibrate and stir, cast into pre-placed molds, and obtain pure gold filling materials. Cut the pure gold filling material into small pieces, which is conve...
Embodiment 3
[0033] Firstly prepare the filling material, mix according to weight ratio, dysprosium 70.0%, indium 12.4%, zinc block 9.0%, cobalt powder 8.6%, cobalt powder average diameter is 20mm. Two metals, dysprosium and indium, are placed in a graphite crucible, and zinc block and cobalt powder are placed in the interlayer of the furnace top in two compartments. Vacuum to 5*10 after closing the furnace door -3 Pa, and then filled with argon, the pressure is 0.8 atmospheres. Melt the dysprosium-indium binary alloy in proportion under the protection of an inert atmosphere. The melting temperature reaches 1480°C to completely melt the binary alloy, then lower the power to reduce the melt temperature to 1120°C, quickly add zinc block and cobalt powder in sequence, and place the crucible Vibrate and stir, cast into pre-placed molds, and obtain pure gold filling materials. Cut the filling material into small pieces, which is convenient for batching.
[0034] The second step is to smelt h...
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