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Vacuum melting method for nickel-aluminum intermetallic compound

An intermetallic compound and vacuum smelting technology, which is applied in the field of material processing, can solve the problems of powder performance influence, difficulty in melting, and short smelting time, etc., and achieve the effect of smooth pouring

Inactive Publication Date: 2017-06-13
QINGDAO R & D INST XIAN JIAOTONG UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the powder used in 3D printing is generally obtained by vacuum casting into ingots after smelting, followed by secondary smelting and atomization to make powder, and in the process of vacuum smelting and pouring, the purity of the alloy melt is guaranteed. The product performance in the follow-up milling and even 3D printing process is very important. The vacuum melting currently used is generally carried out in the crucible of the induction furnace through vacuum induction melting and then pouring. However, the raw materials used for nickel-aluminum intermetallic compounds contain relatively high There are many solid inclusions, which are difficult to melt during the smelting process, and at the same time, it is difficult to float to the surface due to the short melting time. In the ingot, it will affect the performance of the powder produced

Method used

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Embodiment Construction

[0024] The present invention will be further described below in combination with specific embodiments.

[0025] The selected alloy components include Al: 20-30%, Cr: 2-2.8%, Nb: 1.5-2.5%, Re: 0.2-0.8%, and the balance is Ni,

[0026] After converting the above components into mass percentages, select nickel blocks and aluminum blocks corresponding to mass parts, polish off the surface oxide film of aluminum, clean the surface oil, and then use acetone to ultrasonically clean, and weigh the rest of the trace element components for backup use.

[0027] Put the nickel block and the aluminum block into the crucible of the vacuum induction melting furnace. There is a secondary feeding hopper above the crucible, and the trace elements are put into the bin of the secondary feeding hopper.

[0028] The bottom of the crucible is provided with a base that is sealed with the bottom of the crucible. There is a liquid outlet in the center of the base. There are inert gas pipes on both sid...

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Abstract

The invention discloses a vacuum melting method for a nickel-aluminum intermetallic compound. The vacuum melting method comprises the steps that raw materials are selected and added into a crucible and a secondary charging hopper respectively, inert gas pipes at the bottom of the crucible are used for argon blowing after the raw materials are heated, reasonable argon blowing moments and pressure are selected, the alloy liquid is ensured to be stirred by gas in the smelting process so as to become boiling, gas bubbles are formed and carry inclusions which are not easy to melt in the alloy to float up to reach the surface of the alloy liquid, the pressure is gradually reduced in the pouring process, and meanwhile, an uppermost metal liquid which is about 3cm deep finally and enriched in inclusion is left in the crucible.

Description

technical field [0001] The invention belongs to the technical field of material processing, and in particular relates to a vacuum melting method for nickel-aluminum intermetallic compounds. Background technique [0002] Intermetallic Ni 3 Al has abnormal yield strength-temperature effect, as well as high wear resistance and corrosion resistance. It has become an important structural material in the contemporary aerospace industry, civil industry and other fields, especially in the field of aeroengine blades. prospect. 3D printing, or additive manufacturing, is a rapid prototyping process that has emerged in recent years. It adopts layer-by-layer powder coating, laser or electron beam melting and molding to realize the finishing molding of precision parts and avoid the occurrence of defects in the casting process. Defects such as shrinkage cavity and porosity have become a new material processing method. [0003] At present, the powder used in 3D printing is generally obta...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C1/02C22B9/04
CPCC22B9/04C22C1/023
Inventor 张建勋余钊辉徐甄真王茜
Owner QINGDAO R & D INST XIAN JIAOTONG UNIV