Mesoporous carbon material preparation method
A technology of mesoporous carbon and sodium-potassium alloy, which is applied in the preparation/purification of carbon, etc., can solve the problems that it is difficult to meet the requirements of synthetic substances, and the chemical and physical properties of carbon materials are quite different.
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[0028] Chemical materials are: metal sodium, metal potassium, carbon tetrachloride, toluene, ethanol, deionized water, and the preparation dosage of the combination is as follows: in grams and milliliters
[0029]
[0030] (1) Selected chemical substances and materials
[0031] The chemical substances and materials used in the preparation should be carefully selected and their quality and purity should be controlled:
[0032]
[0033] (2) Preparation of sodium potassium alloy
[0034] Weigh 0.4g±0.03g of sodium metal and 1.6g±0.04g of potassium metal, stir for 1min to form a sodium-potassium alloy;
[0035] (3) Synthesis of mesoporous carbon materials at room temperature
[0036] The synthesis of mesoporous carbon materials is carried out under the protection of nitrogen, and is completed by stirring at room temperature;
[0037] ① Prepare mixed reaction mixture
[0038] Weigh 1.2±0.04g of carbon tetrachloride, 1.8±0.05g of sodium potassium alloy, and 200mL±0.5mL of ...
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