Mesoporous carbon material preparation method

A technology of mesoporous carbon and sodium-potassium alloy, which is applied in the preparation/purification of carbon, etc., can solve the problems that it is difficult to meet the requirements of synthetic substances, and the chemical and physical properties of carbon materials are quite different.

Active Publication Date: 2017-06-23
SHENYANG NORMAL UNIV
View PDF2 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In the process of synthesizing carbon materials with organic small molecules or polymers as precursors, most of them need to be calcined and carbonized at high temperature under an inert atmosphere. Due to the different chemical substances selected, the different synthesis parameters, and the differenc

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Mesoporous carbon material preparation method
  • Mesoporous carbon material preparation method
  • Mesoporous carbon material preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Chemical materials are: metal sodium, metal potassium, carbon tetrachloride, toluene, ethanol, deionized water, and the preparation dosage of the combination is as follows: in grams and milliliters

[0029]

[0030] (1) Selected chemical substances and materials

[0031] The chemical substances and materials used in the preparation should be carefully selected and their quality and purity should be controlled:

[0032]

[0033] (2) Preparation of sodium potassium alloy

[0034] Weigh 0.4g±0.03g of sodium metal and 1.6g±0.04g of potassium metal, stir for 1min to form a sodium-potassium alloy;

[0035] (3) Synthesis of mesoporous carbon materials at room temperature

[0036] The synthesis of mesoporous carbon materials is carried out under the protection of nitrogen, and is completed by stirring at room temperature;

[0037] ① Prepare mixed reaction mixture

[0038] Weigh 1.2±0.04g of carbon tetrachloride, 1.8±0.05g of sodium potassium alloy, and 200mL±0.5mL of ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention relates to a mesoporous carbon material preparation method, and belongs to the technical field of preparation and applications of a carbon material. Compared with the background art, the mesoporous carbon material preparation method has obvious progresses, a small organic molecule is taken as a carbon source, a Na-K alloy is taken as a reducing agent, methylbenzene is taken as a solvent, the materials are stirred at the room temperature to prepare a reaction solution, the reaction solution is subjected to suction filtration, washing and vacuum drying to prepare a mesoporous carbon material, the process of the preparation method is advanced, the data are full and accurate, the preparation is fast, high-temperature calcination is not needed, the product is a black powder, the black powder has a mesoporous porous structure, the yield of the product is as high as 75.6%, the mesoporous carbon material can be matched with various chemical substances, and the preparation method is a quite ideal method for preparing the mesoporous carbon material.

Description

technical field [0001] The invention relates to a method for preparing a mesoporous carbon material, which belongs to the technical field of preparation and application of carbon materials. Background technique [0002] Mesoporous carbon materials have good structural adjustability and stability, which is unmatched by other materials. Mesoporous carbon materials have high specific surface area and large pore volume, and have been obtained in the fields of adsorption, catalysis, optics, and electricity. widely used. [0003] The synthesis method and process of mesoporous carbon materials will directly affect the structural characteristics and properties of the material. For example, the choice of template and precursor is the decisive factor. The reaction temperature, solvent, ratio of reactants, pH value of the reaction system, roasting Temperature can also play an important role. [0004] Templating agent is the basic component of synthesizing mesoporous carbon materials....

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C01B32/05
CPCC01P2002/82C01P2004/04C01P2006/17C01P2006/80
Inventor 汤兑海赵震朱君江张文婷
Owner SHENYANG NORMAL UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap