Automatic transmission fluid composition and automatic transmission fluid
A technology of automatic transmission fluid and composition, applied in the direction of lubricating composition, petroleum industry, etc., can solve the problem of mineral oil pour point, oxidation stability, low-temperature viscosity, viscosity-temperature characteristics that cannot fully meet the requirements of automatic transmission fluid, synthetic base oil Complicated preparation process, high price of automatic transmission fluid, etc., to achieve excellent low-temperature flow performance, excellent viscosity-temperature characteristics, and low production cost
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Embodiment 1
[0045] Preparation of polyethylene
[0046] Ethylene homopolymerization uses a 200mL stainless steel high-pressure polymerization kettle equipped with a mechanical stirring paddle and a temperature control device, vacuumizes and replaces nitrogen three times, then vacuumizes, introduces ethylene gas, and adds TaCl under ethylene atmosphere 5 (108mg, 0.30mmol), promoter EtAlCl 2 0.3mL (1mol / L) of hexane solution, selectivity improver AlCl 3 (3.0mmol) and solvent chlorobenzene 10ml. Heat to 60°C, continuously add ethylene at a pressure of 4 MPa, and switch the ethylene atmosphere to hydrogen after stirring at 60°C for 8 hours. After the reactant is completely hydrogenated, the autoclave is evacuated to normal pressure, and a small amount of ethanol is added to deactivate the catalyst. After the reaction solution was concentrated, it was passed through a short column of silica gel to obtain 6.3 g of oily hyperbranched polyethylene. The weight average molecular weight of the oi...
Embodiment 2
[0050] Preparation of polyethylene
[0051] Ethylene homopolymerization uses a 200mL stainless steel high-pressure polymerization kettle equipped with a mechanical stirring paddle and a temperature control device, vacuumizes and replaces nitrogen three times, then vacuumizes, introduces ethylene gas, and adds TaCl under ethylene atmosphere 5 (108mg, 0.30mmol), promoter EtAlCl 2 0.45mL (1mol / L) of hexane solution, selectivity improver AlCl 3 (3.0mmol) and solvent chlorobenzene 10ml. Heat to 60°C, continuously add ethylene at a pressure of 4 MPa, and switch the ethylene atmosphere to hydrogen after stirring at 60°C for 8 hours. After the reactant is completely hydrogenated, the autoclave is evacuated to normal pressure, and a small amount of ethanol is added to deactivate the catalyst. The reaction solution was concentrated and passed through a short column of silica gel to obtain 8.3 g of oily hyperbranched polyethylene. The weight average molecular weight of the oily hyperb...
Embodiment 3
[0055] Preparation of polyethylene
[0056] Ethylene homopolymerization uses a 200mL stainless steel high-pressure polymerization kettle equipped with a mechanical stirring paddle and a temperature control device, vacuumizes and replaces nitrogen three times, then vacuumizes, introduces ethylene gas, and adds TaCl under ethylene atmosphere 5 (144mg, 0.40mmol), promoter EtAlCl 2 0.45mL (1mol / L) of hexane solution, selectivity improver AlCl 3 (3.0mmol) and solvent chlorobenzene 10ml. Heat to 60°C, continuously add ethylene at a pressure of 6 MPa, and switch the ethylene atmosphere to hydrogen after stirring at 60°C for 8 hours. After the reactant is completely hydrogenated, the autoclave is evacuated to normal pressure, and a small amount of ethanol is added to deactivate the catalyst. The reaction solution was concentrated and passed through a short column of silica gel to obtain 8.1 g of oily hyperbranched polyethylene. The weight-average molecular weight of the oily hyperb...
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