Preparation method for material for high-sensitively intelligent regulating humidity
An intelligent and sensitive technology, applied in the direction of color-changing fluorescent materials, chemical instruments and methods, fiber chemical characteristics, etc., can solve the problems of many steps, lack of effective methods for water release, unfavorable large-area preparation, etc., and achieve the effect of high sensitivity
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[0028] A method for preparing a highly sensitive and intelligent humidity control material, comprising the following steps:
[0029] The first step is to synthesize hydroxyethylindole;
[0030] Such as figure 1 As shown in (1), the first step includes the following steps, adding 2,3,3-trimethylindole and 2-bromoethanol into the reaction solvent according to the molar mass ratio of 1:1 for reaction, Reflux for 12 hours. After the reaction, the solvent was evaporated, and the obtained solid product was washed with anhydrous ether for several times to finally obtain a white solid, i.e. isethylindole.
[0031] In the first step, the reaction solvent is acetonitrile, and the evaporation is to use a rotary evaporator to evaporate the solvent.
[0032] Such as figure 1 Shown in (2), the second step, the synthesis of nitrogen hydroxyethyl spiropyran; Said second step comprises the following steps, the hydroxyethylindole synthesized in the first step and 5-nitrosalicylaldehyde and ...
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