Preparation method of pecan shell active carbon
A hickory shell and activated carbon technology, applied in chemical instruments and methods, inorganic chemistry, non-metallic elements, etc., can solve the problems of high equipment requirements, ecological damage, energy consumption, etc., to protect the ecological environment, low cost, and easy to operate. Effect
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Embodiment 1
[0020] After crushing the pecan shells, bake them at 105°C for 100 minutes, then soak them in a phosphoric acid solution with a concentration of 25% by weight, and filter them with a weight ratio of 1:2 between the pecan shells and the phosphoric acid solution; place the filtered residue in a muffle Heating and activating in a furnace, the activation temperature is 300°C, the time is 60min, and then cooled to room temperature to obtain the activated product; the activated product is pickled with 3wt% dilute hydrochloric acid, washed with water until neutral, and finally passed through a 100-mesh sieve to obtain Hickory shell activated carbon, yield 69%.
[0021] According to the experiment, the iodine adsorption value of hickory shell activated carbon is 798mg / g, and the decolorization power of methylene blue is 110mL / g.
Embodiment 2
[0023] After crushing the pecan shells, bake them at 110°C for 80 minutes, then soak them in a phosphoric acid solution with a concentration of 30wt%, and filter them with a weight ratio of 1:3 between the pecan shells and the phosphoric acid solution; put the filtered residue in a muffle Heating and activating in a furnace, the activation temperature is 350°C, the time is 50min, and then cooled to room temperature to obtain the activated product; the activated product is pickled with 4wt% dilute hydrochloric acid, washed with water until neutral, and finally passed through a 100-mesh sieve to obtain Hickory shell activated carbon, the yield is 61%.
[0024] According to the experiment, the iodine adsorption value of hickory shell activated carbon is 812mg / g, and the decolorization power of methylene blue is 109mL / g.
Embodiment 3
[0026] After crushing the hickory nut shells, bake them at 120°C for 60 minutes, then soak them in a phosphoric acid solution with a concentration of 35wt%, and filter them in a weight ratio of 1:4 between the hickory shells and the phosphoric acid solution; put the filtered residue in a muffle Heating and activating in the furnace, the activation temperature is 400°C, the time is 30min, and then cooled to room temperature to obtain the activated product; the activated product is pickled with 5wt% dilute hydrochloric acid, washed with water until neutral, and finally passed through a 100-mesh sieve to obtain Hickory shell activated carbon, yield 53%.
[0027] According to the experiment, the iodine adsorption value of hickory shell activated carbon is 803mg / g, and the decolorization power of methylene blue is 123mL / g.
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