Polypropylene carbonate moisture-curable polyurethane hot-melt adhesive and preparation method thereof
A polypropylene carbonate and polyurethane hot melt adhesive technology, applied in the direction of polyurea/polyurethane adhesives, adhesives, adhesive types, etc., can solve problems such as poor mechanical properties, limitations, and low glass transition temperature, and achieve Effect of Good Adhesive Properties
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Embodiment 1
[0027] Take 50 parts of polypropylene carbonate (Mn=2000) and 50 parts of polytetrahydrofuran ether glycol (Mn=2000) into the reaction kettle, dehydrate at 110°C for 2 hours; cool to 60°C, fill with nitrogen, and take 20 parts Diphenylmethane diisocyanate was slowly added to the reaction kettle, and then the temperature was slowly raised. The temperature was controlled at 110°C while reacting for 2 hours under the protection of nitrogen; after the reaction, 0.1 part of dibutyltin dilaurate was added, and then pumped at 110°C. Vacuum until no bubbles appear, then discharge the material and seal the package.
[0028] According to the test method, the tensile shear strength of the adhesive to stainless steel, aluminum, PC, PMMA, and ABS are 3.93MPa, 3.67MPa, 5.54MPa, 3.81MPa, and 1.71MPa, respectively.
Embodiment 2
[0030] Take 25 parts of polypropylene carbonate (Mn=2000), 25 parts of polyhexylene adipate glycol (Mn=2000), and 50 parts of polytetrahydrofuran ether glycol (Mn=2000) into the reaction kettle. Dehydrate at 110°C for 2 hours; cool to 60°C, fill with nitrogen protection, slowly add 20 parts of diphenylmethane diisocyanate to the reactor, then slowly increase the temperature, control the temperature at 110°C, and react for 2 hours under nitrogen protection; After the completion, add 0.1 part of dibutyl tin dilaurate, then vacuumize at 110°C until no bubbles appear, then discharge the material and seal the package.
[0031] According to the test method, the tensile shear strength of the adhesive to stainless steel, aluminum, PC, PMMA, and ABS is 2.86 MPa, 2.41 MPa, 5.78 MPa, 3.62 MPa, and 1.65 MPa, respectively.
Embodiment 3
[0033] Take 50 parts of polypropylene carbonate (Mn=2000) and 50 parts of polyethylene adipate diol (3000) into the reaction kettle, dehydrate at 110°C for 1.5 hours; cool to 60°C, and fill with nitrogen for protection, Take 18 parts of diphenylmethane diisocyanate slowly into the reactor, then slowly increase the temperature, control the temperature at 120℃, and react for 3.5 hours under nitrogen protection, then vacuum at 110℃ until no bubbles appear, and then discharge the material sealed package.
[0034] According to the test method, the tensile shear strength of the adhesive to iron, stainless steel and aluminum are 7.50MPa, 5.22MPa, and 5.09MPa, respectively.
[0035] Note: Examples 1 to 3, after the adhesive is prepared, when bonding the substrates (iron, stainless steel, aluminum, PC, PMMA, ABS), the bonding process is as follows: first turn on the heating system and set the temperature to 90-120℃, let the synthesized adhesive be heated at this temperature for 10-30 minut...
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