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Laminated and film-coated anti-reflection glass and preparation method thereof

A technology of anti-reflection glass and anti-reflection film, which is applied in the direction of coating, etc., can solve the problems of limitation of film material and coated parts, unsuitability for outdoor environment, complicated preparation process, etc., and achieve good film uniformity, short preparation process, good matching effect

Active Publication Date: 2017-09-05
北京冠华东方玻璃科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, these preparation processes are relatively complicated, the process conditions are also complex, the required equipment is expensive, and there are certain restrictions on the film material and the plated parts, the cost is high, and it is not suitable for outdoor environments.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A method for preparing laminated coating anti-reflection glass, characterized in that the specific preparation steps are as follows:

[0028] (1) Put the glass substrate into a beaker with ethanol solution and ultrasonically clean it for 40 minutes, then rinse it with deionized water; then place the glass substrate in a certain concentration of acid solution for 10 seconds, then rinse it with deionized water; After cleaning, place the glass substrate in an oven at 60°C to dry for later use; the acid is sulfuric acid with a mass concentration of 10%;

[0029] (2) Place the pretreated glass substrate in step (1) in the quartz tube reaction chamber; start the mechanical pump to evacuate the reaction chamber, and inject N 2 Wash 5 times;

[0030] (3) Coat the silica gel on the glass substrate, feed the preheated reaction gas, turn on the vacuum pump, and dry the silica gel at 50°C to form a silica airgel membrane isolation layer;

[0031] (4) Introduce SiH on the isolatio...

Embodiment 2

[0036] A method for preparing laminated coating anti-reflection glass, characterized in that the specific preparation steps are as follows:

[0037] (1) Put the glass substrate in a beaker filled with ethanol solution for ultrasonic cleaning for 20 minutes, then rinse with deionized water; then place the glass substrate in an acid solution of a certain concentration for 10 seconds, and then rinse with deionized water; After cleaning, place the glass substrate in an oven at 60°C to dry for later use; the acid is hydrochloric acid with a mass concentration of 3% to 10%;

[0038](2) Place the pretreated glass substrate in step (1) in the quartz tube reaction chamber; start the mechanical pump to evacuate the reaction chamber, and inject N 2 Wash 3 times;

[0039] (3) Coat the silica gel on the glass substrate, feed the preheated reaction gas, turn on the vacuum pump, and dry the silica gel at 60°C to form a silica airgel membrane isolation layer;

[0040] (4) Introduce SiH on t...

Embodiment 3

[0045] A method for preparing laminated coating anti-reflection glass, characterized in that the specific preparation steps are as follows:

[0046] (1) Put the glass substrate into a beaker with ethanol solution and ultrasonically clean it for 30 minutes, then rinse it with deionized water; then place the glass substrate in a certain concentration of acid solution for 30 seconds, then rinse it with deionized water; After cleaning, place the glass substrate in an oven at 60°C to dry for later use; the acid is hydrofluoric acid with a mass concentration of 3%;

[0047] (2) Place the pretreated glass substrate in step (1) in the quartz tube reaction chamber; start the mechanical pump to evacuate the reaction chamber, and inject N 2 Wash 10 times;

[0048] (3) Coat the silica gel on the glass substrate, feed the preheated reaction gas, turn on the vacuum pump, and dry the silica gel at 80°C to form a silica airgel membrane isolation layer;

[0049] (4) Introduce SiH on the isol...

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Abstract

The invention relates to laminated and film-coated anti-reflection glass and a preparation method thereof. The laminated and film-coated anti-reflection glass is prepared from a glass substrate, and an isolation layer, an anti-dazzling light film layer and a visible light anti-reflection film layer which are arranged on the glass substrate, wherein the isolation layer is a silicon dioxide aerogel film; the anti-dazzling light film layer is a porous-structure film layer obtained by corroding tin oxide through utilizing acid; the visible light anti-reflection film layer is a fluorine-doped composite film layer of titanium dioxide, niobium oxide, zirconium oxide, tin oxide and zinc oxide. Lamination and film coating are adopted; especially, the isolation layer is designed to be the silicon dioxide aerogel film and light is subjected to diffuse reflection for a plurality of times through micro-pores in the isolation layer; the tin oxide porous-structure film layer is designed on the anti-dazzling light film layer and the visible light anti-reflection film layer is the fluorine-doped composite film layer, so that light reflection is reduced and emitted light is reduced to be 1 percent or lower; a new technical way is explored for the anti-reflection glass and is suitable for industrial application.

Description

technical field [0001] The invention relates to a coated glass, in particular to a low-radiation anti-reflection coated glass and a manufacturing method thereof. Background technique [0002] We all have the experience of being disturbed by glare in our daily life. In 1984, the Illuminating Engineering Society of North America defined glare as: the feeling of annoyance, discomfort or loss of visual performance caused by lighting far larger than the eyes can adapt to within the field of vision. It refers to the overflowing light that causes discomfort to the human body, which is serious light pollution. Glare is a visual condition, which is formed either due to improper brightness distribution, or too large a range of brightness changes, or extreme contrast in space and time, which causes discomfort or reduces the importance of observation. The ability of an object, or both phenomena at the same time. Glare can be caused by high-brightness light sources (lights, sunlight) ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C17/34
CPCC03C17/3417C03C2217/213C03C2217/23C03C2217/73C03C2218/112C03C2218/152
Inventor 陈庆司文彬曾军堂
Owner 北京冠华东方玻璃科技有限公司
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