Water-soluble PVA (polyvinyl alcohol) fiber as well as preparation method and application thereof
A fiber and dissolution temperature technology, applied in the chemical characteristics of fibers, chemical instruments and methods, rayon manufacturing, etc., can solve problems such as formation pollution and use restrictions, and achieve the effects of reducing damage, reducing dosage, and good degradable performance.
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Embodiment 1
[0039] Embodiment 1: prepare water-soluble PVA fiber, main steps are as follows:
[0040] (1) Preparation of spinning stock solution: the degree of polymerization is 1600, the degree of alcoholysis is 95.0 (mol)% PVA and boric acid are dissolved in water and made into spinning stock solution, the mass concentration of PVA in the stock solution is 15%, boric acid is added The amount is 0.5% of the PVA mass, the stock solution is heated up to 105 ° C, and the pressure is maintained at 0.08 MPa, dissolved for 12 hours, then filtered, defoamed, and then enters the spinning process.
[0041] (2) Spinning: The PVA stock solution is sent to the spinning assembly by a metering pump, and the PVA stock solution is sprayed into the coagulation bath from the small hole of the spinneret. The composition of the coagulation bath is dimethyl sulfoxide and ethanol, the mass ratio of dimethyl sulfoxide and ethanol is 5:18, the temperature of the coagulation bath is 15°C, and the PVA stays in th...
Embodiment 2-10
[0044] Example 2-10: Referring to Example 1, operate according to the parameters in the following Attached Table 1 and Attached Table 2 to prepare Example 2-10. Explanation: In Attached Table 1 and Attached Table 2, DP means degree of polymerization, Ad means degree of polyvinyl alcoholysis, unit (mol / mol)%.
[0045] Schedule 1:
[0046]
[0047] Schedule 2:
[0048]
[0049]
Embodiment 11
[0051] This embodiment provides a fiber-containing guar gum fracturing fluid, the preparation method of which is as follows:
[0052] Step 1: under stirring condition, add 0.2 weight part of thickener hydroxypropyl guar gum (China Petroleum Substances Kunshan Company), 0.12 weight part of sodium carbonate, 0.1 weight part of potassium chloride to 100 weight parts of water, then stir for 20min, Obtain guar thickener aqueous solution;
[0053] Step 2: under stirring conditions, add 0.2 parts by weight of crosslinking agent aluminum nitrate to the above-mentioned thickener aqueous solution to obtain guar gum fracturing fluid (excluding fiber guar gum fracturing fluid);
[0054] Step 3: Add 0.5 parts by weight of the PVA fiber prepared in Example 1 to the above-mentioned guar gum fracturing fluid, cut the fiber to a length of 10 mm, add it to the oil and gas field fracturing fluid and disperse evenly, and obtain the fiber-containing guar gum fracturing fluid.
[0055] Step 4: Add...
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