Preparation method of lube base oil
A lubricating oil base oil and raw material oil technology, which is applied in chemical instruments and methods, petroleum industry, and hydrocarbon oil treatment, can solve the problems of different catalyst combinations and loading methods that are rarely reported, and achieve the effect of increasing yield
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[0031] The present invention provides a method for preparing lubricating base oil. The method includes: contacting feedstock oil with at least two isomerization catalysts including molecular sieve and group VIII noble metals in a reactor and performing a hydroisomerization reaction to obtain Lubricating oil base oil; wherein, according to the flow direction of the feedstock oil, at least two isomerization catalysts in the reactor are set such that the diameter of the isomerization catalyst located downstream is larger than the diameter of the isomerization catalyst located upstream path.
[0032] According to the present invention, according to the flow direction of the feedstock oil (the feedstock oil can flow from top to bottom, from bottom to top, or alternately from top to bottom), at least two isomerization catalysts can be filled in the reactor by filling only one reactor , Multiple reactors can also be packed; if only one reactor is packed, one bed can be packed with only ...
Example
[0072] Preparation Example 1
[0073] (1) Take 30g (on a dry basis, the same below) ZSM-12 molecular sieve (twelve-membered ring molecular sieve, with a silicon-to-aluminum ratio of 80) and 70g (on a dry basis, the same below) alumina (based on the Provided in the form of boehmite, the same below) is prepared by dry mixing and extruding into a cylindrical wet strip with a diameter of 1.4 mm. The wet bar was dried at 120°C for 4 hours, and then calcined at 500°C for 6 hours to obtain a catalyst carrier. The water absorption of the catalyst carrier was determined to be 0.9. The measurement method of water absorption is: put 100g carrier in a beaker, add 2 times deionized water to soak for 2h, filter out excess water and weigh the wet bar, subtract 100g from the wet bar weight and divide by 100 to obtain the water absorption rate .
[0074] (2) Dissolve 2.29g zinc nitrate hexahydrate in water, then add water to make the volume up to 100mL. The resulting solution was used to impreg...
Example
[0077] Preparation Example 2
[0078] The method of Preparation Example 2 is basically the same as that of Preparation Example 1, except that the diameter of the cylindrical wet bar in step (1) is 1.6 mm, and the catalyst B-2 prepared in Preparation Example 2 is shown in the composition Table 1.
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