Intelligent label for indicating freshness of aquatic products and preparation method of intelligent label
A smart label and freshness technology, which is applied in the direction of material analysis, measuring devices, instruments, etc. by observing the impact on chemical indicators, can solve the problem of low sensitivity, achieve good intuitiveness, realize fine management, and high sensitivity Effect
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[0038] In the preparation method of the smart label of the present invention, the pretreatment step includes 3 PO 4 :H 2 SO 4 :HNO 3 The volume ratio of 7:2:1, the chemical polishing step at 95~110℃ for 1~2min.
[0039] In the preparation method of the smart label of the present invention, in the primary anodizing step, the electrolyte uses a 0.4mol / L phosphoric acid solution, the oxidation voltage is 100V, the oxidation time is 120min, and the oxidation temperature is 0-4°C.
[0040] The method for preparing the smart label of the present invention is characterized in that the chemical etching step is etching in a mixed acid solution of 6% phosphoric acid and 1.8% chromic acid for 6-10 hours, and the temperature is controlled at 50-60°C.
[0041] In the preparation method of the smart label of the present invention, in the aluminum removal step, a mixed solution of saturated copper sulfate aqueous solution and hydrochloric acid with a volume ratio of 3:1 is used.
[0042] The smart la...
Example Embodiment
[0049] Example 1: Preparation of Anodic Aluminum Oxide Film (AAO)
[0050] (1) Sample pretreatment
[0051] Cut the aluminum sheet into small circles with a diameter of 25 mm, and soak them in acetone for 30 minutes to remove oil stains. At room temperature, soak in 0.1mol / L NaOH solution and ultrasonic for 5 minutes to remove the natural oxide film on the surface, and then clean it with deionized water. Finally in the mixed acid (H 3 PO 4 , H 2 SO 4 , HNO 3 , Volume ratio 7:2:1), chemical polishing at 95~110℃ for 1~2min.
[0052] (2) Primary anodic oxidation
[0053] The pretreated aluminum sheet is sandwiched between two thin plates, and placed in an oxidation tank for aluminum anodization. The electrolyte uses 0.4mol / L phosphoric acid solution, the oxidation voltage is 100V, the oxidation time is 120min, and the oxidation temperature is 0. ~4℃. The platinum sheet is used as the cathode, and the aluminum sheet is used as the anode. The sample adopts CP8-600V arc oxidation power s...
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