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Wheat bran oil production technology using subcritical butane extraction

A wheat bran and production technology technology, which is applied in the directions of fat oil/fat production, fat production, etc., can solve the problems of no extraction rate, high wheat bran oil extraction process, etc., and achieves the effects of high extraction rate and simple process

Inactive Publication Date: 2017-11-10
QILU UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In order to make up for the deficiencies of the prior art and solve the problem that the prior art does not have a wheat bran oil extraction process suitable for industrial application with a simple process and a high extraction rate, the present invention provides a production method for subcritical butane extraction of wheat bran oil. craft

Method used

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  • Wheat bran oil production technology using subcritical butane extraction
  • Wheat bran oil production technology using subcritical butane extraction
  • Wheat bran oil production technology using subcritical butane extraction

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Experimental program
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Effect test

Embodiment 1

[0028] 1 Experimental materials and equipment

[0029] 1.1 Experimental materials

[0030] Wheat bran (large flakes) commercially available

[0031] 1.2 Experimental reagents

[0032] Butane: Henan Xinxiang Xinyang Steel Cylinder Co., Ltd.

[0033] Sodium methoxide, HCl-methanol solution, anhydrous sodium sulfate: commercially available, all analytically pure;

[0034] n-Hexane: commercially available, chromatographically pure

[0035] 1.3 Experimental Instruments

[0036] CBE-30+5L subcritical fluid extraction laboratory complete set of equipment: Henan Subcritical Biotechnology Co., Ltd.

[0037] JZC-30TSE electronic balance: Fuzhou Kedi Electronic Technology Co., Ltd.

[0038] Agilent GCMS (GC7890b+MS5977b): Agilent Corporation of the United States

[0039] Syringe microporous membrane filter (□13mm, pore size 0.45μm): Changzhou Ruikang Medical Equipment Co., Ltd.

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Abstract

The invention discloses a wheat bran oil production technology using subcritical butane extraction, and belongs to the field of food engineering. Wheat bran undergoes subcritical butane extraction multiple times, and the obtained extract liquid undergoes reduced pressure distillation to remove an extractant to obtain the wheat bran oil containing methyl palmitate, methyl linoleate and methyl oleate. The wheat bran is cyclically extracted by adopting a subcritical butane technology, and technologic optimization researches of factors affecting the yield of the wheat bran oil are carried out by adopting Box-Benhnken center combination response surface test design in order to obtain optimum technologic parameters; and a gas chromatograph-mass spectrometer (GC-MS) is used to analyze the fatty acid components of the wheat bran oil obtained through the subcritical extraction in order to provide reference for the development and the utilization of wheat bran resources. The wheat bran oil production technology is simple, allows the extraction rate to reach up to 86.92%, is suitable for industrial application, and provides a new way for the further utilization of the wheat bran.

Description

technical field [0001] The invention relates to the field of food engineering, in particular to a production process for subcritical butane extraction of wheat bran oil. Background technique [0002] Wheat bran is the residual part after extracting wheat flour and germ in the milling process, which accounts for 14% to 19% of the wheat mass. Bran contains rich amylase, protein, phytic acid and other active compounds, and has very prominent If the bran can be fully utilized for deep processing and comprehensive utilization, it will have high economic and social benefits. [0003] In recent years, studies on wheat bran extract at home and abroad have shown that wheat bran extract can effectively control blood sugar and reduce the risk of cardiovascular disease in diabetic patients; regulate the effectiveness and retention of minerals; activate the body to use selenium as The main oxidative stress protection mechanism; various physiological functions such as anti-tumor and immu...

Claims

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Application Information

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IPC IPC(8): C11B1/10
CPCC11B1/10C11B1/108
Inventor 张志国田鑫
Owner QILU UNIV OF TECH
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