Functionally graded carbides
A functional gradient and carbide technology, applied in chemical instruments and methods, crystal growth, metal layered products, etc., can solve problems such as low feed rate and uninterrupted cutting
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[0070] Tantalum carbide monoliths were fabricated from ζ-Ta 4 C 3-x Formed, with dimensions 4 x 3 x 45 mm, as specified in ASTM Standard C-1161-02, Measurement of Flexural Strength of Advanced Ceramics. ζ-Ta 4 C 3-x The monolith was processed by hot pressing and contained 95% by weight ζ-Ta 4 C 3-x . Rod specimens were supported on one end and the long face was exposed to hydrogen and 5% methane (CH 4 ) for a fixed period of time in the range of 10-20 hours to carburize the specimen.
[0071] Carburized samples were characterized by three techniques. (a) Evaluation of the microstructure on etched cross-sections near the carburized surface using an optical microscope (model: MEF4M, Leica, Wein, Austria). (b) An X-ray diffractometer (XRD, model Philips X'Pert-MPD, PANalytical Inc., Westborough, MA) and associated software was used to identify crystalline phases and estimate the weight percent of phases in the substrate and carburized surface. (c) Using a Knoop microhard...
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