Preparation technique for medical titanium alloy small-diameter thick-wall pipe
A preparation process and technology for thick-walled pipes, which are applied in metal rolling, manufacturing tools, metal rolling, etc., can solve the problems of high processing viscosity, low processing yield and high price of titanium alloys, and achieve good biocompatibility. , the effect of promoting regeneration and improving, good mechanical properties
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Embodiment 1
[0027] A preparation process of a medical titanium alloy small-diameter thick-walled tube, comprising the following steps:
[0028] Step A1: Using the vacuum consumable arc melting method to prepare an ultra-low gap medical titanium alloy ingot, forging the titanium alloy ingot to make a round ingot, and then cross-rolling an ultra-low gap titanium alloy tube billet on a cross-rolling piercer, The diameter of the ultra-low gap titanium alloy round ingot is Φ 40-60mm, the diameter of the ultra-low gap titanium alloy tube blank is Φ 45-65mm, and the wall thickness is 15-20mm;
[0029] Step B1: After heating the tube billet, use a planetary rolling mill to roll it into a thick-walled tube billet. The mandrel is made of tungsten alloy during rolling. The temperature for heating the tube billet is 700-1000 ° C. Thick-walled pipe blank, the diameter of the thick-walled pipe blank after rolling is Φ20-30mm, and the wall thickness is 6-10mm. Due to the high rolling temperature of tita...
Embodiment 2
[0035] A pure titanium medical small-diameter thick-walled titanium alloy pipe with a diameter of 6 mm and a wall thickness of 2 mm was prepared.
[0036] Step A2: Prepare ultra-low-gap medical pure ingots by using vacuum consumable arc melting method, forge and open the pure titanium ingots to make Φ40mm round ingots, and cross-roll ultra-low-gap titanium alloy tube blanks on a cross-rolling piercer. Billet diameter is Φ45mm, wall thickness is 15mm;
[0037] Step B2: After heating the pure titanium tube blank at 700°C, roll it into a thick-walled tube blank with a planetary rolling mill, the tube diameter is Φ 20mm, the wall thickness is 6mm, and the mandrel is made of tungsten alloy during rolling;
[0038] Step C2: Heat the thick-walled pipe blank rolled by the planetary rolling mill, and after heating, use the H13 steel rod with a layer of tin on the outer layer as the core rod, the thickness of the tin coating is 100 μm, and insert it The inner hole of the wall pipe blank ...
Embodiment 3
[0043] A TA18 titanium alloy medical small-diameter thick-walled titanium alloy pipe with a diameter of 10 mm and a wall thickness of 4 mm was prepared.
[0044] Step A3: Prepare the ultra-low gap medical TA18 titanium alloy ingot by using the vacuum consumable arc melting method, forge and open the TA18 titanium alloy ingot to make a Φ50mm round ingot, and cross-roll the ultra-low gap TA18 titanium alloy on the cross-rolling piercer Tube blank, tube blank diameter is Φ55mm, wall thickness is 18mm;
[0045] Step B3: After heating the TA18 titanium alloy tube billet to 800°C, use a planetary rolling mill to roll it into a thick-walled tube billet with a diameter of Φ25mm and a wall thickness of 8mm. The mandrel is made of tungsten alloy during rolling;
[0046] Step C3: Heat the thick-walled pipe blank rolled by a planetary rolling mill. After heating, use a Hastelloy C-276 high-temperature alloy rod with a layer of aluminum hot-coated on the outer layer as a core rod. Put the...
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