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Preparation technique for medical titanium alloy small-diameter thick-wall pipe

A preparation process and technology for thick-walled pipes, which are applied in metal rolling, manufacturing tools, metal rolling, etc., can solve the problems of high processing viscosity, low processing yield and high price of titanium alloys, and achieve good biocompatibility. , the effect of promoting regeneration and improving, good mechanical properties

Inactive Publication Date: 2017-12-08
SHENZHEN YUANSIDACHENG TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Because the inner hole of the hollow bone screw is very small, the processing technology of short solid titanium alloy bar is mainly used in China, and then the external thread is turned. Due to the high viscosity of titanium alloy, when drilling with a small diameter drill, it is often Drilling is off-center, resulting in waste products, low processing yield, and large-scale industrial production cannot be realized
In foreign countries, thick-walled titanium alloy pipes of about 3m are directly prepared, with good concentricity, and directly enter the machining center to turn titanium alloy bone nails, so the yield and processing efficiency are very high. However, due to the technical blockade of foreign countries, my country is currently unable to manufacture The thick-walled titanium alloy pipe with a length of 3m makes foreign thick-walled titanium alloy pipes expensive, and the domestic bone nails cannot be produced efficiently, which eventually makes the bone nails remain high, causing a heavy medical burden on surgical patients in our country

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A preparation process of a medical titanium alloy small-diameter thick-walled tube, comprising the following steps:

[0028] Step A1: Using the vacuum consumable arc melting method to prepare an ultra-low gap medical titanium alloy ingot, forging the titanium alloy ingot to make a round ingot, and then cross-rolling an ultra-low gap titanium alloy tube billet on a cross-rolling piercer, The diameter of the ultra-low gap titanium alloy round ingot is Φ 40-60mm, the diameter of the ultra-low gap titanium alloy tube blank is Φ 45-65mm, and the wall thickness is 15-20mm;

[0029] Step B1: After heating the tube billet, use a planetary rolling mill to roll it into a thick-walled tube billet. The mandrel is made of tungsten alloy during rolling. The temperature for heating the tube billet is 700-1000 ° C. Thick-walled pipe blank, the diameter of the thick-walled pipe blank after rolling is Φ20-30mm, and the wall thickness is 6-10mm. Due to the high rolling temperature of tita...

Embodiment 2

[0035] A pure titanium medical small-diameter thick-walled titanium alloy pipe with a diameter of 6 mm and a wall thickness of 2 mm was prepared.

[0036] Step A2: Prepare ultra-low-gap medical pure ingots by using vacuum consumable arc melting method, forge and open the pure titanium ingots to make Φ40mm round ingots, and cross-roll ultra-low-gap titanium alloy tube blanks on a cross-rolling piercer. Billet diameter is Φ45mm, wall thickness is 15mm;

[0037] Step B2: After heating the pure titanium tube blank at 700°C, roll it into a thick-walled tube blank with a planetary rolling mill, the tube diameter is Φ 20mm, the wall thickness is 6mm, and the mandrel is made of tungsten alloy during rolling;

[0038] Step C2: Heat the thick-walled pipe blank rolled by the planetary rolling mill, and after heating, use the H13 steel rod with a layer of tin on the outer layer as the core rod, the thickness of the tin coating is 100 μm, and insert it The inner hole of the wall pipe blank ...

Embodiment 3

[0043] A TA18 titanium alloy medical small-diameter thick-walled titanium alloy pipe with a diameter of 10 mm and a wall thickness of 4 mm was prepared.

[0044] Step A3: Prepare the ultra-low gap medical TA18 titanium alloy ingot by using the vacuum consumable arc melting method, forge and open the TA18 titanium alloy ingot to make a Φ50mm round ingot, and cross-roll the ultra-low gap TA18 titanium alloy on the cross-rolling piercer Tube blank, tube blank diameter is Φ55mm, wall thickness is 18mm;

[0045] Step B3: After heating the TA18 titanium alloy tube billet to 800°C, use a planetary rolling mill to roll it into a thick-walled tube billet with a diameter of Φ25mm and a wall thickness of 8mm. The mandrel is made of tungsten alloy during rolling;

[0046] Step C3: Heat the thick-walled pipe blank rolled by a planetary rolling mill. After heating, use a Hastelloy C-276 high-temperature alloy rod with a layer of aluminum hot-coated on the outer layer as a core rod. Put the...

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Abstract

The invention relates to the field of material preparation, in particular to a preparation technique for a medical titanium alloy small-diameter thick-wall pipe. The preparation technique comprises the following steps that (A) a super-low-gap medical titanium alloy circle-forming bar is prepared, and a super-low-gap titanium alloy pipe blank is formed through skew rolling; (B) the super-low-gap titanium alloy pipe blank is heated and then rolled into a thick-wall pipe blank through a tungsten alloy planetary rolling mill; (C) the thick-wall pipe blank is heated, and a heat-resistance rod serves as a core rod and is inserted in an inner hole of the thick-wall pipe blank and placed in a rotary swaging machine to subjected to rotary swaging to form a small-diameter pipe, wherein a low melting point material is hot-plated on the outer layer of the heat-resistance rod; and (D) the small-diameter pipe and the core rod are heated till the temperature reaches the melting temperature of the low melting point material, and through a core-pulling machine, the heat-resistance rod serving as the core rod is pulled out. Compared with the prior art, the preparation technique for the medical titanium alloy small-diameter thick-wall pipe is simple and high in production efficiency, and the cast ingot specification and the titanium alloy material are wide in adaptation range.

Description

【Technical field】 [0001] The invention relates to the field of material preparation, in particular to a preparation process of a medical titanium alloy small-diameter thick-walled tube. 【Background technique】 [0002] In recent years, titanium alloys have been more and more widely used in the biomedical field. The compound growth rate of the global orthopedic implant devices and implant materials market in the past five years is about 10.4%. In 2015, it has reached 27.7 billion US dollars. The market has reached 16.6 billion yuan, with a compound annual growth rate of 18.1%. The Chinese market has become the focus of the world. It has become the second largest market country in the world in terms of the number of operations, the number of products, and the market value of products. The demand for high-quality medical devices Demand is steadily increasing. [0003] Biomaterials currently used in bone repair are not only required to replace damaged tissues, but also have good...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B21C37/06B21B25/00
CPCB21B25/00B21C37/06
Inventor 金鹏卢卓梁贺
Owner SHENZHEN YUANSIDACHENG TECH
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