Micron fiber/nano fiber composited electret filter material and preparation method thereof
A microfiber and nanofiber technology, applied in filtration and separation, membrane filters, fiber treatment, etc., can solve the problems of reducing the dielectric properties of materials and the impact of long-term charge storage capacity, achieving enhanced charge stability, simple preparation methods, The effect of enhanced charge storage capacity
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Embodiment 1
[0033] A microfiber / nanofiber composite electret filter material and a preparation method thereof. The preparation method mainly includes the following steps: 1) uniformly dispersing hydroxyapatite (addition amount 0.5wt%, particle size 0.05 μm) in N,N- In dimethylformamide, a dispersion liquid was formed. After ultrasonic stirring for 0.5 hours, polyvinylidene fluoride (weight average molecular weight: 320,000) was added to the dispersion liquid, and after sealing, it was placed in a 60°C water bath and heated and stirred for 10 hours. Finally, a stable and uniform polymer spinning solution A with a mass concentration of 20wt% is prepared for preparing the nanofiber layer;
[0034] Similarly, hydroxyapatite (addition amount 1wt%, particle size 0.05 μm) was uniformly dispersed in N, N-dimethylformamide to form a dispersion liquid, and after ultrasonic stirring for 0.5 h, polystyrene (weight average The molecular weight is 80,000) into the dispersion, and after sealing, it is c...
Embodiment 2
[0040] A microfiber / nanofiber composite electret filter material and a preparation method thereof. The preparation method mainly includes the following steps: 1) uniformly dispersing hydroxyapatite (0.5wt% added, 0.1μm particle size) in N,N- In dimethylacetamide, a dispersion liquid was formed, and after ultrasonic stirring for 0.5 h, polyvinylidene fluoride (weight average molecular weight: 570,000) was added to the dispersion liquid, and after sealing, it was placed in a 60°C water bath and heated and stirred for 8 hours. Finally, a stable and uniform polymer spinning solution A with a mass concentration of 18wt% is prepared for preparing the nanofiber layer;
[0041] Similarly, hydroxyapatite (addition amount 1wt%, particle size 0.05 μm) was uniformly dispersed in N, N-dimethylformamide to form a dispersion liquid, and after ultrasonic stirring for 0.5 h, polystyrene (weight average The molecular weight is 80,000) into the dispersion, and after sealing, it is continuously s...
Embodiment 3
[0047] A microfiber / nanofiber composite electret filter material and a preparation method thereof. The preparation method mainly includes the following steps: 1) uniformly dispersing polytetrafluoroethylene (addition amount 0.05wt%, particle size 0.2 μm) in N,N- In dimethylacetamide, a dispersion liquid was formed. After ultrasonic stirring for 1 hour, polyvinylidene fluoride (weight-average molecular weight: 570,000) was added to the dispersion liquid. After sealing, put it into a 60°C water bath and heat and stir for 8 hours. Finally, It is prepared into a stable and uniform polymer spinning solution A with a mass concentration of 18wt%, which is used to prepare a nanofiber layer;
[0048] Similarly, polytetrafluoroethylene (addition amount 0.1wt%, particle size 0.2 μm) was uniformly dispersed in N, N-dimethylacetamide to form a dispersion liquid, and after ultrasonic stirring for 0.5 h, polysulfone (weight average The molecular weight is 70,000) into the dispersion, and aft...
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