Tea leaf-sourced plant soft capsule shell and application and preparation method of tea leaf-sourced plant soft capsule
A soft capsule shell and soft capsule technology, which are applied in the directions of capsule delivery, cosmetic preparations, skin care preparations, etc., can solve the problems of easy leakage of gelatin capsule shells, adhesion and cross-linking reactions, and high pollution risks, so as to overcome the product Defects, not easy to deform and stick, overcome the effect of easy leakage
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[0029] Example 1,
[0030] Refer to figure 1 , The method for preparing a tea plant soft capsule in the embodiment of the present invention includes the following main steps in sequence:
[0031] a) Preparation of tea extract: the picked tea leaves are washed, dried, crushed, and passed through a 40-mesh sieve to obtain tea powder. The tea powder is 1:40 (w / v, g / ml) and 0.06mol / L sodium hydroxide The solution is evenly mixed, that is, 40 ml of 0.06mol / L sodium hydroxide solution is added to each 1 gram of tea powder; the extract is leached in a water bath at 90-100°C for 60 min, and the extract is shaken every 5 min; Adjust the pH to 5.8 with hydrochloric acid to obtain a tea extract.
[0032] b) Modified tea fiber preparation: take 5g of tea residues washed to neutrality and dried by hot air in a three-necked flask with a stirring device, add 50ml of 75% ethanol, 50ml of 20% NaOH solution, and alkalization temperature of 30℃. The alkalization reaction was carried out at 200r / min ...
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[0035] Example 2,
[0036] In the embodiment of the present invention, the enzymatic hydrolysis treatment process is adopted for the tea dregs after the tea leaves are leached, and the rest of the preparation method is basically the same as in embodiment 1, the difference is:
[0037] a) Enzymatic hydrolysis of tea dregs: Mix 20% NaOH (or 2% dilute sulfuric acid solution) solution with the tea dregs after washing to neutrality and drying 10:1, (10mL of liquid corresponds to 1g of solid) in a water bath at 120℃. After boiling for 30 minutes, filter and wash until neutral. Add 2g of tea dregs fiber and 100U of cellulase washed to neutrality into a 250ml flask with stopper, then add 100ml of 0.2mol / L HAc-NaAc buffer with a pH of 4.8, and place it under constant temperature shaking In the vessel, react at 50°C for 24 to 48 hours. After the enzymatic hydrolysis is completed, the tea dregs are filtered out, the enzymatic hydrolysate is incorporated into the tea extract, and the next st...
Example Embodiment
[0039] Example 3.
[0040] Preparation of the soft capsule described in the embodiment of the present invention has different enzymatic hydrolysis methods for the tea residue fiber, and other preparation processes are basically the same as in Example 2. In this embodiment, the cellulase of the enzymatically hydrolyzed tea dregs is adjusted to one or more of a multi-enzyme system such as polygalacturonase, β-glucosidase, pectinase, and protease to act synergistically.
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