Warm mixed colorized synthetic asphalt, mixture containing warm mixed colorized synthetic asphalt and their preparation methods
A technology of asphalt mixture and colored asphalt, which is applied in petroleum wax refining, climate change adaptation, petroleum wax recovery, etc., and can solve problems affecting the color and service life of colored asphalt, thermal aging of colored asphalt, high-temperature cracking, etc.
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Embodiment 1
[0075] (A) Preparation of warm mix agent
[0076] Including (1) hydroconversion and (2) sweating.
[0077] (1) Hydroconversion
[0078] Using the wax oil product (n-paraffin content: 95.5wt%; drop melting point: 86.2°C; penetration (25°C) 55 dmm) from the low-temperature F-T synthesis experimental device of China Petroleum & Chemical Corporation as raw material, the FHJ-2 catalyst ( A Ni / Al 2 o 3 Commercial catalyst, developed and produced by Fushun Petrochemical Research Institute, with an active metal content of 40% in terms of oxides, and the catalyst is subjected to conventional reduction treatment before use), under the action of reaction pressure 6.5MPa, reaction temperature 220°C, volume space velocity 1.0h -1 Hydrogenation is carried out under the condition of 500:1 volume ratio of hydrogen to liquid to convert olefins and oxygenates therein.
[0079] Properties of hydrogenation products: n-paraffin weight content 97.36%; drop melting point 85.0°C; penetration (25...
Embodiment 2
[0104] (A) Preparation of warm mix agent
[0105] This embodiment includes: (1) hydroconversion and (2) sweating.
[0106] (1) Hydroconversion
[0107] Using the wax oil product (n-paraffin content: 90.0wt%; drop melting point: 82.6°C; penetration (25°C) 62 dmm) from the low-temperature F-T synthesis experimental device of China Petroleum & Chemical Corporation as raw material, the catalyst (Mo-Ni / Al 2 o 3 , the active metal content is 20% in terms of oxides), under the action of reaction pressure 3.0MPa, reaction temperature 300℃, volume space velocity 2.0h -1 Hydrogenation is carried out under the condition of 100:1 volume ratio of hydrogen to liquid to convert olefins and oxygenates therein.
[0108] Properties of hydrogenation products: n-paraffin weight content 93.3%; drop melting point 80.6°C; penetration (25°C) 65 dmm; chromatography-mass spectrometry analysis, no alcohol, alkene, acid and other substances were detected.
[0109] It can be seen that the oxygenate...
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