Preparation method of biodegradable copolyester hot melt adhesive
A biodegradable, copolyester technology, used in adhesives and other directions, can solve problems such as the impact of degradable properties, and achieve good bonding effect
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[0015] Example 1:
[0016] A method for preparing biodegradable copolyester by hot melt, the steps are as follows:
[0017] (1) Dibasic acid composed of 166g terephthalic acid, 66.4g isophthalic acid, 34.5g dodecanedioic acid and 10.1g sebacic acid is composed of 177.3g butanediol and 44.84g 1 , 3-propanediol composed of diol, and a catalyst composed of 0.0107g of tetrabutyl titanate and 0.0107g of antimony acetate, added to the 1L esterification reactor, the reaction temperature is 160℃~205℃, when the ester When the amount of distilled water in the chemical reaction kettle is 95% or more of the theoretical amount of water, the esterification reaction ends;
[0018] (2) Add 1.3345g of the 1010 antioxidant to the product of step (1), carry out the polycondensation reaction for 2.0h under the conditions of 230℃~240℃, 100Pa~150Pa, and then release the vacuum with nitrogen. Get it out of heat.
[0019] The product prepared by Example 1 is labeled A1.
Example Embodiment
[0020] Example 2:
[0021] A method for preparing biodegradable copolyester by hot melt, the steps are as follows:
[0022] (1) Add the dibasic acid and diol as in Example 1, and the catalyst composed of 0.019g tetrabutyl titanate and 0.0237g antimony acetate into a 1L esterification reactor. The reaction temperature 160°C~205°C, when the amount of distilled water in the esterification reactor is 95% or more of the theoretical amount of water, the esterification reaction ends;
[0023] (2) Add 1.6014g of the 1010 antioxidant to the product of step (1), and carry out the polycondensation reaction for 2.0h under the conditions of 230℃~240℃, 100Pa~150Pa, and then release the vacuum with nitrogen. Get it out of heat.
[0024] The product prepared in Example 2 is labeled A2.
Example Embodiment
[0025] Example 3:
[0026] A method for preparing biodegradable copolyester by hot melt, the steps are as follows:
[0027] (1) Add the dibasic acid and dihydric alcohol as in Example 1 and the catalyst composed of 0.0295g of tetrabutyl titanate and 0.0185g of antimony acetate into a 1L esterification reactor. The reaction temperature 160°C~205°C, when the amount of distilled water in the esterification reactor is 95% or more of the theoretical amount of water, the esterification reaction ends;
[0028] (2) Add 1.8683g of 1010 antioxidant to the product of step (1), carry out the polycondensation reaction for 2.0h under the conditions of 230℃~240℃, 100Pa~150Pa, and then release the vacuum with nitrogen. Get it out of heat.
[0029] The product prepared in Example 3 is labeled A3.
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