Preparation method of edible packaging film based on diatom polysaccharide
A diatom polysaccharide and packaging film technology, applied in packaging, packaging paper, transportation and packaging, etc., can solve the problems of plastic packaging materials increasing the environmental burden, secondary pollution of main soil and water resources, and incompatible with low-carbon economic development. , to achieve the effects of simple and feasible preparation method, good application value and market potential, and easy industrial scale production
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Embodiment 1
[0013] The preparation method of the edible packaging film based on diatom polysaccharide comprises the degreasing of diatom powder, the preparation of diatom polysaccharide, and the preparation of edible packaging film. The specific steps are:
[0014] 1) Diatom powder degreasing: Add chloroform-methanol mixture to diatom powder at a weight ratio of 1:8, the volume ratio of chloroform and methanol in the mixture is 2.5:1, degrease at 50°C for 4 hours, repeat the operation twice , suction filtered, and dried at 50°C to obtain degreased diatom powder, which is set aside;
[0015] 2) Preparation of diatom polysaccharide: mix defatted diatom powder and water evenly according to the ratio of material to liquid of 1:18, then add 8-chlorophylline, and extract under ultra-high pressure for 5 minutes at a temperature of 60°C and a pressure of 200MPa. Suction filtration, the filter residue was treated twice in the same way, the filtrate was combined to obtain water to extract the crude...
Embodiment 2
[0018] The preparation method of the edible packaging film based on diatom polysaccharide comprises the degreasing of diatom powder, the preparation of diatom polysaccharide, and the preparation of edible packaging film. The specific steps are:
[0019] 1) Diatom powder degreasing: Add chloroform-methanol mixture to diatom powder at a weight ratio of 1:11, the volume ratio of chloroform and methanol in the mixture is 1.5:1, degrease at 60°C for 2 hours, repeat the operation 3 times , suction filtered, and dried at 40°C to obtain degreased diatom powder, which is set aside;
[0020] 2) Preparation of diatom polysaccharide: mix defatted diatom powder and water evenly according to the ratio of material to liquid 1:22, then add 8-chlorophylline, and extract at ultra-high pressure for 2 minutes at a temperature of 50°C and a pressure of 400MPa. Suction filtration, the filter residue was treated 3 times in the same way, the filtrate was combined to obtain water to extract the crude ...
Embodiment 3
[0023] The preparation method of the edible packaging film based on diatom polysaccharide comprises the degreasing of diatom powder, the preparation of diatom polysaccharide, and the preparation of edible packaging film. The specific steps are:
[0024] 1) Diatom powder degreasing: Add chloroform-methanol mixture to diatom powder at a weight ratio of 1:10, the volume ratio of chloroform and methanol in the mixture is 2.0:1, degrease at 55°C for 3 hours, repeat the operation 3 times , suction filtered, and dried at 45°C to obtain defatted diatom powder, which is set aside;
[0025] 2) Preparation of diatom polysaccharide: mix defatted diatom powder and water evenly according to the ratio of material to liquid 1:20, then add 8-chlorophylline, and extract under ultra-high pressure for 4 minutes at a temperature of 55 °C and a pressure of 300 MPa. Suction filtration, the filter residue was treated 3 times in the same way, the filtrate was combined to obtain water to extract the cr...
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