Organic chemical synthesis reactor capable of being integrally operated

Abstract

The invention relates to an organic chemical synthesis reactor capable of being integrally operated. The organic chemical synthesis reactor capable of being integrally operated comprises a reaction bottle, a reaction bottle cover, a reaction bottle heating device, an ultrasonic sprayer, an xenon lamp, a temperature-measuring and cooling device, an extracting device, an eluant preparation device, achromatographic column separating device and a receiving bottle, wherein the reaction bottle cover is arranged on the top of the reaction bottle and is sealed with the reaction bottle; the reaction bottle heating device is arranged on the bottom and / or the side part of the reaction bottle; the ultrasonic sprayer is communicated with the inner part of the reaction bottle; the xenon lamp and the temperature-measuring and cooling device respectively penetrate into the reaction bottle from the reaction bottle cover; the extracting device is arranged on the bottom of the reaction bottle and is communicated with the inner part of the reaction bottle; the extracting device and the eluant preparation device separately communicate with the chromatographic column separating device; and the chromatographic column separating device is communicated with the receiving bottle. The organic chemical synthesis reactor has the advantages of being capable of performing separation of solid products, liquid products and gas-phase products, saving organic synthesis experiment time and reducing waste of reaction raw materials and energy consumption loss.

Description

technical field [0001] The invention belongs to the technical field of organic chemical synthesis, relates to an organic chemical synthesis reactor, in particular to an organic chemical synthesis reactor capable of integrated operation. Background technique [0002] With the rapid development of chemical technology and the gradual maturity of organic chemical synthesis technology, organic synthesis has been able to synthesize organic compounds from simple compounds or elements through chemical reactions. Urea was synthesized in the 1830s; in the second half of the 19th century, a variety of Dye; in the 1940s, DDT, organophosphorus insecticides, organosulfur fungicides, herbicides and other pesticides were synthesized; at the beginning of the 20th century, 606 agents were synthesized; in the 1930s and 1940s, more than a thousand sulfonamide compounds were synthesized. The synthesis and use of these organic compounds play a vital role in daily life, industrial and agricultural...

AI Technical Summary

Problems solved by technology

However, only the synthetic reaction part is involved, and the further separation and purification of the synthetic product is not involved. At the same time, the light source of the synthetic reaction part does not give a specific type of light.

Existing organic synthesis reactions either use light alone or use heating for synthesis, and do not involve the combination of light and heating under microwave-assisted synthesis conditions for an integrated synthesis reaction, and the synthesis reaction part and the product separation part are both In order to carry out separately, the operation process will be more complicated, which will inevitably cause waste of energy and test time

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