Method for synthesizing phenylalanyl-lysine dipeptide
A technology of lysine dipeptide and phenylalanyl is applied in the field of peptide synthesis to achieve the effects of mild conditions, huge social value and economic benefits, and high synthesis efficiency
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0029] A method for synthesizing phenylalanyl-lysine dipeptide, its specific process steps are as follows:
[0030] (1) Preparation of phenylalanine and lysine aqueous solution
[0031] Dissolve an appropriate amount of commercially available phenylalanine and lysine in a pure aqueous solution successively under stirring to prepare an aqueous solution with a phenylalanine concentration of 0.3mol / L and a lysine concentration of 0.3mol / L; Sodium hydroxide adjusts the pH value of the aqueous solution to 7.5, that is, an aqueous solution of phenylalanine and lysine is prepared, which is used in the next step to prepare an ethylene glycol non-aqueous reaction medium.
[0032] (2) Preparation of ethylene glycol non-aqueous reaction medium
[0033] After the (1) step was completed, the phenylalanine and lysine aqueous solution prepared in the (1) step were mixed with ethylene glycol solution, wherein the volume ratio of phenylalanine and lysine aqueous solution to ethylene glycol 1...
Embodiment 2
[0047] A method for synthesizing phenylalanyl-lysine dipeptide, its specific process steps are as follows:
[0048] (1) Preparation of phenylalanine and lysine aqueous solution
[0049] Dissolve an appropriate amount of commercially available phenylalanine and lysine in a pure aqueous solution successively under stirring to prepare an aqueous solution with a concentration of phenylalanine of 0.6mol / L and a concentration of lysine of 1.2mol / L; Sodium hydroxide adjusts the pH value of the aqueous solution to 8.5, that is, an aqueous solution of phenylalanine and lysine is prepared, which is used in the next step to prepare an ethylene glycol non-aqueous reaction medium.
[0050] (2) Preparation of ethylene glycol non-aqueous reaction medium
[0051] After the (1) step was completed, the phenylalanine and lysine aqueous solution prepared in the (1) step were mixed with ethylene glycol solution, wherein the volume ratio of phenylalanine and lysine aqueous solution to ethylene gly...
Embodiment 3
[0065] A method for synthesizing phenylalanyl-lysine dipeptide, its specific process steps are as follows:
[0066] (1) Preparation of phenylalanine and lysine aqueous solution
[0067] Dissolve an appropriate amount of commercially available phenylalanine and lysine in a pure aqueous solution successively under stirring to prepare an aqueous solution with a phenylalanine concentration of 1.0mol / L and a lysine concentration of 2.0mol / L; Sodium hydroxide adjusts the pH value of the aqueous solution to 9.5, that is, an aqueous solution of phenylalanine and lysine is prepared, which is used in the next step to prepare an ethylene glycol non-aqueous reaction medium.
[0068] (2) Preparation of ethylene glycol non-aqueous reaction medium
[0069] After the (1) step was completed, the phenylalanine and lysine aqueous solution prepared in the (1) step were mixed with ethylene glycol solution, wherein the volume ratio of phenylalanine and lysine aqueous solution to ethylene glycol 1...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com