Spray containing melaleuca alternefolia hydrosol and preparation method of spray
A technology of Melaleuca alternifolia and spray, which is applied in the directions of medical preparations containing active ingredients, preparations for skin care, pharmaceutical formulations, etc., can solve the problem of insufficient research on the remaining substances in Melaleuca alternifolia
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preparation Embodiment 1
[0034] Preparation Example 1: Preparation of Spray
[0035] Dissolve the compound of formula I in water, add other solvents, stabilizers and emulsifiers in sequence, fully shake until clarified, filter, and package. The solvent is selected from one or more of water, glycerin, propylene glycol and ethanol; the stabilizer is selected from one or more of Span, lauryl alcohol and colloidal silicon dioxide; the emulsifier is selected from emulsifiers temperature. Wherein the addition amount of the compound of formula I does not exceed 0.5% of the total amount. Those skilled in the art can understand that any method for preparing sprays in the prior art can prepare the sprays of the present invention, which are all simple improvements to the sprays of the present invention
preparation Embodiment 2
[0036] Preparation Example 2: Preparation of Formula I Compound
[0037] (1) Get 500 grams of leaves of fresh Melaleuca alternifolia, pulverize, put into a distillation tower, heat and pressurize distillation, separate, and recycle extract to obtain pure dew; those skilled in the art can know that the pure dew preparation process is the present Known in the art, those skilled in the art can adopt any other pure dew extraction method, and this all is the simple improvement to the method of the present invention.
[0038] (2) Mix the pure dew in step (1) with ethanol at a mass ratio of 1:8, stir at a constant temperature of about 55°C for 6 hours, and decoct 3 times for 2 hours each time;
[0039] (3) Combine the decoction liquids, filter and concentrate until the relative density at 80° C. is about 1.2, and a pale yellow oily liquid is obtained.
[0040] (4) Use silica gel column chromatography on the light yellow oily liquid, wash with ethanol+water mixed solvent gradient with ...
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