Tooth filling and repairing material and preparation method thereof

A technology for repairing materials and teeth, which is applied in dental preparations, dentistry, dental prostheses, etc., and can solve problems such as poor physical and mechanical properties, damaged restoration edge seals, micro-leakage, etc.

Active Publication Date: 2018-05-11
北京安泰生物医用材料有限公司 +1
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  • Summary
  • Abstract
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] The current composite resin products still have certain deficiencies: 1) There is volume shrinkage during the curing of the composite resin monomer, which may not fit tightly with the cavity wall, resulting in microleakage or secondary caries; 2) The loss of anatomical form due to material wear still remains It is a common problem in composite resin restorations; 3) There is still a certain difference between the optical refractive index of composite resin and human teeth, resulting in a visible dividing line between the restoration material and the tooth interface, which affects the appearance
The inorganic fillers in existing composite resins are generally quartz fillers, which have a large contact angle with water, low water absorption reduces micro-leakage, and have strong surface pollution resistance, but relatively poor physical and mechanical properties
At the same time, the composite resin has a certain degree of polymerization shrinkage, and the polymerization shrinkage of the composite resin seriously damages the edge seal of the restoration and causes the bonding of the tooth restoration interface to be damaged.
There are also many limitations in the existing preparation methods, such as: the process is too complicated, the cycle is long, and the operability is poor

Method used

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  • Tooth filling and repairing material and preparation method thereof
  • Tooth filling and repairing material and preparation method thereof
  • Tooth filling and repairing material and preparation method thereof

Examples

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Effect test

Embodiment 1-4

[0093] The raw materials and dosages used in Examples 1-4 are shown in Table 1; wherein, the dosage of each component is calculated according to the mass fraction of the components in the dental filling restoration material.

[0094] The preparation method of embodiment 1-4 dental filling restorative material is the same, and the specific preparation method is as follows:

[0095] (1) Preparation of pre-polymerized resin powder: Bis-GMA resin monomer and initiator benzoyl peroxide (BPO) are mixed, and the consumption of benzoyl peroxide is 0.2% of Bis-GMA resin quality, stirs at 50 ℃ 5hr, exhaust for 15min to make the vacuum degree -0.1Mpa. After the stirring is completed, pour it into the tray, the thickness of the material is 10-20mm, and cover the tray with aluminum foil. After the pouring was completed, the tray was put into an oven for polymerization, the polymerization initiation temperature was 65° C., and the polymerization time was 5 hours. After the polymerization ...

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Abstract

The invention discloses a tooth filling and repairing material and a preparation method thereof, and belongs to the technical field of tooth materials. The tooth filling and repairing material includes a resin matrix, an adjuvant, a filler, and pre-polymerized resin powder. The pre-polymerized resin powder is formed by polymerization of Bis GMA (bisphenol A diglycidyl methacrylate). The preparation method of the tooth filling and repairing material comprises the following steps: preparation of the pre-polymerized resin powder, mixing of the resin matrix and the adjuvant, mixing of a mixture Aand the filler, and mixing of a mixture B and the pre-polymerized resin powder. The tooth filling and repairing material prepared by the method has bending strength of 80-120 MPa after curing, compressive strength of 200-300 MPa and shrinkage rate of 1.3-2%. Compared with the prior art, the tooth filling and repairing material has good comprehensive mechanical properties and low shrinkage rate, and is suitable for industrial mass production.

Description

technical field [0001] The invention belongs to the technical field of tooth materials, and in particular relates to a tooth filling restoration material and a preparation method thereof. Background technique [0002] 1. About the condition of the teeth [0003] 1.1 Dental diseases [0004] With the changes in the lifestyle of human society and the aging of the social population, the incidence of tooth erosion in adolescents and tooth and face caries in the elderly is increasing year by year. At present, the incidence rate of tooth erosion among teenagers is as high as 60%. Epidemiological investigations show that the incidence rate of a certain university population in Beijing is 45.8%. According to the third national oral health epidemiological survey report, the caries rate of 65-74-year-old people in my country is 98.4%, and the root caries rate is as high as 63.6%. The further development of these two types of dental hard tissue diseases will lead to pulp inflammatio...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K6/083
CPCA61K6/887C08L35/02
Inventor 冯广辉陈科斌陈思坦姜昊王琪王晓燕于鹏袁重阳
Owner 北京安泰生物医用材料有限公司
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