A precision oscillating reaction device for material preparation

Abstract

The invention discloses a precise vibration reaction device for material production. The device comprises an outer cylinder, the inner wall of the outer cylinder is fixedly provided with a vacuum detector, a barrel cap is hinged to the outside top of the outer cylinder, the vacuum detector is connected with a vacuum pump through a first control module, the barrel cap comprises an upper cap and a lower cap, a round slot is arranged in the bottom surface of the lower cap, a light emitting module and a light receiving module are fixedly arranged in two slot walls of the round slot, the light receiving module is connected with a hydraulic vibrator through a second control module, an inner cylinder is arranged at the top of the hydraulic vibrator through a vibrating rod, the inner wall of the inner cylinder is fixedly provided with a temperature measuring module, and the temperature measuring module is connected with a heater through a third control module. A preparation nano-material is overturned and vibrated through the vibration of the inner cylinder in order to accelerate the reaction rate, and the detection and the control of the vacuum pump, the hydraulic vibrator and the heaterthrough various detection modules and the control module makes a reaction carried out at a high rate in order to greatly improve the yield and the quality of the nano-material.

Description

technical field [0001] The invention relates to the technical field of nanomaterial reaction devices, in particular to a precision oscillation reaction device for material preparation. Background technique [0002] Adding nano-materials to the production of PVC pipes to enhance the use effect. Nanotechnology is a brand-new comprehensive science and technology. When substances are "crushed" to the nanometer level and made into nanomaterials, not only the properties of light, electricity, heat, and magnetism will change, but also have radiation, absorption, catalysis, adsorption, etc. Many new features can greatly change the current industrial structure. Nanotechnology has broad development prospects, and chemically prepared nanomaterials generally require reaction devices to speed up the reaction. The reaction device is a comprehensive reaction vessel, which is used to complete processes such as hydrolysis, neutralization, crystallization, distillation, evaporation, storage,...

AI Technical Summary

Problems solved by technology

[0004] (1) The traditional reaction device is generally equipped with a stirring device. Through stirring, the objects are mixed more uniformly and the reaction is faster. The chemical reaction is completed under the strong stirring of the stirring paddle, but it is easy to cause damage to the crystal structure or molecular structure of the product. , and the stirring of the stirring paddle sometimes produces a stirring dead angle, which affects the quality of the product;

[0005] (2) Before the current oscillating reaction device prepares nanomaterials, although there is a temperature required for the reaction in the device when the material is just put into the device, as the reaction progresses, the temperature will gradually lose, and if the temperature cannot be obtained during the reaction To long-term maintenance, the reaction rate will drop, which will greatly reduce the yield and reduce the yield and quality of nanomaterials.

Images