Oil-based drill cutting continuous microwave pyrolysis device and process

A technology of oil-based drill cuttings and pyrolysis, which is applied in the petroleum industry, pyrolysis treatment of sludge, and treatment of hydrocarbon oil. It can solve the problems of ineffective use of pyrolysis residue heat energy and low microwave absorption efficiency. Uniform distribution, prolonging service life and saving equipment space

Active Publication Date: 2018-06-26
CHINA UNIV OF PETROLEUM (EAST CHINA)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are also problems, such as the use of belt conveyor, the need to install a sludge shape controller to control the sludge shape, the microwave absorption efficiency is low, and the pyrolysis residue and its residual heat energy have not been effectively utilized, etc.

Method used

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  • Oil-based drill cutting continuous microwave pyrolysis device and process
  • Oil-based drill cutting continuous microwave pyrolysis device and process

Examples

Experimental program
Comparison scheme
Effect test

Embodiment example

[0045] Implementation case: Oil-based drill cuttings were dried in Zhejiang Oilfield, with a water content of 5% and an oil content of 4%.

[0046] The oil-based drill cuttings are placed in the continuous microwave pyrolysis equipment of the present invention for pyrolysis reaction. The temperature is increased for 20 min to 500° C. under 900 W power, and the temperature pyrolysis is 30 min. The oil and gas recovery rate is above 90%, and the oil content of the pyrolysis residue is It is 0.28%.

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Abstract

The invention discloses an oil-based drill cutting continuous microwave pyrolysis device. The device comprises a feeding device, a microwave reaction device, an oil and gas cooling recovery device anda pyrolysis residue cooling device. The feeding device comprises a feeding bin and a belt conveyor. The microwave reaction device comprises a microwave reaction chamber, a waveguide feed port is arranged at the top end of the microwave reaction chamber, and a quartz chamber is arranged inside the microwave reaction chamber. The quartz chamber is composed of a fixed ring wall and a rotating tray,and the top end of the quartz chamber is open. A feeding buffer bin is disposed below the end of the belt conveyor and communicated with the quartz chamber through a chute. A discharging port is arranged on the fixed ring wall at the position above the corresponding discharge buffer bin. The discharging port is provided with a scraper plate, and the scraper plate is connected to the discharge buffer bin through a chute. The device can achieve continuous uniform feeding and continuous discharging without blockage in the closed environment, prevents leakage of microwaves, and prolongs service life.

Description

Technical field [0001] The invention relates to a continuous microwave pyrolysis equipment and process for oil-based drill cuttings, belonging to the field of oily solid waste treatment. Background technique [0002] As a key technology for shale gas extraction, oil-based drilling fluids will generate a large amount of hazardous solid wastes such as oil-based drilling cuttings during use. Oil-based drilling fluids have been used because they contain pollutants such as petroleum hydrocarbons, heavy metals, and organics. If it is listed as a national hazardous waste, if it is discharged directly without treatment, it will cause serious harm to the surrounding ecological environment. In this regard, the harmless treatment of oil-based solid waste such as oil-based drill cuttings is imminent. [0003] The pyrolysis technology treatment plan of oily solid waste is to heat it to a certain temperature under anaerobic conditions (usually about 450°C or even higher), so that the hydrocarbo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F11/10C10G1/00
CPCC02F11/10C10G1/002C10G2300/1003Y02W10/40
Inventor 侯影飞游海鹏齐升东黄朝琦张瑶瑶赵朝成牛青山
Owner CHINA UNIV OF PETROLEUM (EAST CHINA)
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