Preparation method for adsorbing material for lysine

An adsorption material and lysine technology, applied in the field of adsorbent preparation, can solve the problems of complicated operation, long consumption time, etc., and achieve the effects of large adsorption capacity, firm adhesion, and not easy to be broken.

Inactive Publication Date: 2018-06-29
孝感市锐思新材科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The existing lysine production or purification process mostly adopts the method of crystallization or ion exchange for purification in the purification process, which has the disadvantages of long time consumpt

Method used

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  • Preparation method for adsorbing material for lysine

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0029] Example 1

[0030] Step 1. Prepare the enhanced adsorption composition, each portion represents 1Kg mass, and its composition is:

[0031] Component parts by weight

[0032] Component parts by weight

[0033] White oil 100 parts

[0034] Styrene 3 parts

[0035] 0.5 part of methylcyclohexene-1,2-dicarboxylic anhydride

[0036] 2 parts of 1-amino-3-butene-2-ol

[0037] 0.3 parts of 2-hydroxyethyl methacrylate phosphate

[0038] 0.3 parts of methacryloyloxyethyl trimellitic anhydride

[0039] 0.007 parts of allyl hexafluoroisopropyl ether

[0040] 0.0003 parts of bis(trimethylenedithio)tetrathiafulvalene

[0041] Step 2. Preparation of lysine adsorption material, each portion represents 1Kg mass, and its composition is:

[0042] Component parts by weight

[0043] Porous glass beads 100 parts

[0044] Enhanced adsorption composition 20 parts

[0045] Polyvinyl alcohol 1 part

[0046] 0.75 parts of ammonium persulfate

[0047] 600 parts of water

[0048] The above components are mixed uniformly, t...

Example Embodiment

[0049] Example 2

[0050] Step 1. Prepare the enhanced adsorption composition, each portion represents 1Kg mass, and its composition is:

[0051] Component parts by weight

[0052] Component parts by weight

[0053] White oil 100 parts

[0054] Styrene 1 part

[0055] 0.2 part of methylcyclohexene-1,2-dicarboxylic anhydride

[0056] 1-amino-3-butene-2-ol 1 part

[0057] 0.1 part of 2-hydroxyethyl methacrylate phosphate

[0058] 0.1 part of methacryloxyethyl trimellitic anhydride

[0059] 0.005 parts of allyl hexafluoroisopropyl ether

[0060] 0.0001 parts of bis(trimethylenedithio)tetrathiafulvalene

[0061] Step 2. Preparation of lysine adsorption material, each portion represents 1Kg mass, and its composition is:

[0062] Component parts by weight

[0063] Porous glass beads 100 parts

[0064] Enhanced adsorption composition 10 parts

[0065] Polyvinyl alcohol 0.5 parts

[0066] Ammonium persulfate 0.5 parts

[0067] 400 parts of water

[0068] The above components are mixed uniformly, the temperat...

Example Embodiment

[0069] Example 3

[0070] Step 1. Prepare the enhanced adsorption composition, each portion represents 1Kg mass, and its composition is:

[0071] Component parts by weight

[0072] White oil 100 parts

[0073] Styrene 5 parts

[0074] 0.6 parts of methylcyclohexene-1,2-dicarboxylic anhydride

[0075] 6 parts of 1-amino-3-butene-2-ol

[0076] 0.5 parts of 2-hydroxyethyl methacrylate phosphate

[0077] 0.5 parts of methacryloxyethyl trimellitic anhydride

[0078] 0.05 parts of propenyl hexafluoroisopropyl ether

[0079] Bis(trimethylenedithio)tetrathiafulvalene 0.001 parts

[0080] Step 2. Preparation of lysine adsorption material, each portion represents 1Kg mass, and its composition is:

[0081] Component parts by weight

[0082] Porous glass beads 100 parts

[0083] Enhanced adsorption composition 30 parts

[0084] 1.5 parts of polyvinyl alcohol

[0085] Ammonium persulfate 1 part

[0086] 800 parts of water

[0087] The above components are mixed uniformly, the temperature is raised to 105° C., an...

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Abstract

The invention relates to a preparation method for an adsorbing material for lysine. According to specific parts by weight, the adsorbing material is prepared from porous glass beads, polyvinyl alcohol, ammonium persulfate, water and an enhanced adsorption composition, which are heated to react, and after the product is processed, the adsorbent product is obtained.

Description

technical field [0001] The invention relates to a preparation method of an adsorbent, in particular to a preparation method of an adsorption material for lysine. Background technique [0002] Lysine is an amino acid needed by the human body, an indispensable nutrient. It is known that protein is the main component of human cells. After entering the human body, protein in food is first decomposed into amino acids after digestion, and then the human body uses these amino acids to synthesize new human proteins, such as immune antibodies, digestive enzymes, plasma proteins, growth Hormones, etc. are all synthesized human proteins. Among the various amino acids in the synthesis of proteins, L-lysine is the most important one. Without it, other amino acids will be restricted or not utilized. Scientists call it the first essential amino acid for the human body. Scientists have also discovered that L-lysine is the most important and essential component of Somatotation (ss), an imp...

Claims

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Application Information

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IPC IPC(8): B01J20/26B01D15/08B01J20/30C08F212/08C08F216/14C08F222/04C08F226/02C08F230/02C08F232/00
CPCB01J20/265B01D15/08B01J20/04C08F212/08C08F226/02C08F230/02C08F232/00C08F222/04C08F216/1408
Inventor 王大可曹东立
Owner 孝感市锐思新材科技有限公司
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