Heat conduction graphene slurry and preparation method thereof
A graphene and graphene aerogel technology, applied in epoxy resin coatings, polyurea/polyurethane coatings, coatings, etc., can solve the problems of weakening the heat dissipation performance of graphene, difficult sintering process, and unsuitable for high temperature processing. , to achieve the effect of improved flexibility, low temperature conditions and easy construction
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Embodiment 1
[0019] The graphene thermally conductive slurry of the present embodiment includes the following components and parts by weight thereof: 1 part of graphene, 0.5 part of graphene airgel anti-settling agent, 0.5 part of binder polyvinylidene fluoride, N-methyl 98 parts of pyrrolidone, wherein, the bulk density of the graphene airgel is 0.01g / cm 3 , porosity 89%, oil absorption 300g / g, electrical conductivity 1500S / m, specific surface area 1650m 2 / g.
[0020] The preparation method of the graphene heat conduction paste described in the present embodiment, comprises the steps:
[0021] (1) Add 0.5 parts of polyvinylidene fluoride to 98 parts of N-methylpyrrolidone, stir well to make a mixed solution;
[0022] (2) Add 1 part of graphene and 0.5 part of graphene airgel to the mixture;
[0023] (3) Use a high-shear disperser to stir the mixed liquid prepared in step (2), the stirring speed is 1000r / min, and the stirring time is 1h, to obtain a stably dispersed thermally conductiv...
Embodiment 2
[0025] The graphene thermally conductive slurry of the present embodiment comprises the following components and parts by weight thereof: 10 parts of graphene, 3 parts of graphene airgel anti-settling agent, 5 parts of binder epoxy resin, N-methylpyrrolidone 82 parts, wherein, the bulk density of the graphene airgel is 0.001g / cm 3 , porosity 99%, oil absorption 600g / g, electrical conductivity 2300S / m, specific surface area 2000m 2 / g.
[0026] The preparation method of the graphene heat conduction paste described in the present embodiment, comprises the steps:
[0027] (1) Add 5 parts of epoxy resin to 82 parts of N-methylpyrrolidone, stir well to make a mixed solution;
[0028] (2) Add 10 parts of graphene and 3 parts of graphene airgel to the mixture;
[0029] (3) Use a high-shear disperser to stir the mixed liquid prepared in step (2), the stirring speed is 8000r / min, and the stirring time is 10h to obtain a stably dispersed thermally conductive slurry with a solid conte...
Embodiment 3
[0031] The graphene thermally conductive slurry of the present embodiment includes the following components and parts by weight: 6 parts of graphene, 2 parts of graphene airgel anti-settling agent, 3 parts of binder polyurethane, and 89 parts of N-methylpyrrolidone , wherein, the bulk density of the graphene airgel is 0.007g / cm 3 , porosity 93%, oil absorption 500g / g, electrical conductivity 1800S / m, specific surface area 2000m 2 / g.
[0032] The preparation method of the graphene heat conduction paste described in the present embodiment, comprises the steps:
[0033] (1) Add 3 parts of polyurethane to 89 parts of N-methylpyrrolidone, stir evenly to make a mixed solution;
[0034] (2) Add 6 parts of graphene and 2 parts of graphene airgel to the mixture;
[0035] (3) Use a high-shear disperser to stir the mixed liquid prepared in step (2), the stirring speed is 6000r / min, and the stirring time is 5h, to obtain a stably dispersed heat-conducting paste, the solid content of w...
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Abstract
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