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Chromogenic film with concave-convex structure, pressure test film and preparation method thereof

A technology of concave-convex structure and pressure testing, applied in hydraulic/pneumatic metering, devices for coating liquids on surfaces, protein coatings, etc.

Active Publication Date: 2022-03-29
BAODING LUCKY INNOVATIVE MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, it is difficult to perform pressure testing with high sensitivity in the case of testing small pressures using a pressure testing membrane

Method used

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  • Chromogenic film with concave-convex structure, pressure test film and preparation method thereof
  • Chromogenic film with concave-convex structure, pressure test film and preparation method thereof
  • Chromogenic film with concave-convex structure, pressure test film and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

example 1

[0069] Base coat slurry preparation

[0070] SBR 6kg

[0071] PVA217(10%) 10kg

[0072] water 84kg

[0073] 6kg of SBR and 10kg of 10% PVA217 aqueous solution were added to 84kg of water, stirred evenly, and prepared as a primer slurry for use.

[0074] Preparation of Concave-convex Structure Layer Coating Solution

[0075] Polyurethane acrylate 40kg

[0076] Epoxy acrylate 20kg

[0077]

[0078] Add 20kg of epoxy acrylate to 40kg of urethane acrylate, stir evenly, then add 25kgPET3A and 15kg DPHA in turn, after stirring evenly, add 3kg184 and 3kgTPO, stir well and prepare the concave-convex structure layer slurry for use.

[0079] Preparation of microcapsules and their dispersions

[0080] Preparation of oil phase solution:

[0081] Diisopropylnaphthalene 60kg

[0082] CVL 3.0kg

[0083] BLMB 2.4kg

[0084] Trimethylolpropane adduct of hexamethylene diisocyanate 12kg

[0085] Methyl ethyl ketone 5kg

[0086] Add 3.0kgCVL and 2.4kgBLMB into 60kg of diisopropylna...

example 2

[0110] Base coat slurry preparation

[0111] SBR 6kg

[0112] PVA217(10%) 10kg

[0113] water 84kg

[0114] 6kg of SBR and 10kg of 10% PVA217 aqueous solution were added to 84kg of water, stirred evenly, and prepared as a primer slurry for use.

[0115] Preparation of Concave-convex Structure Layer Coating Solution

[0116]

[0117] Add 20kg epoxy acrylate to 40kg urethane acrylate, stir evenly, then add 22kgPET3A and 18kgDPHA in turn, after stirring evenly, add 3kg 907 and 3kg TPO, stir well and prepare the concave-convex structure layer slurry for use.

[0118] Preparation of microcapsules and their dispersions

[0119] Preparation of oil phase solution:

[0120] Diisopropylnaphthalene 60kg

[0121] CVL 4.4kg

[0122] BLMB 3.6kg

[0123] Trimethylolpropane adduct of hexamethylene diisocyanate 10kg

[0124] Methyl ethyl ketone 5kg

[0125] Add 4.4kg CVL and 3.6kg BLMB into 60kg diisopropylnaphthalene and 5kg methyl ethyl ketone, stir until completely dissolved, a...

example 3

[0149] Base coat slurry preparation

[0150] SBR 5kg

[0151] PVA117(10%) 15kg

[0152] water 80kg

[0153] Add 5kg of SBR and 15kg of 10% PVA117 aqueous solution into 80kg of water, stir evenly, and prepare the undercoating slurry for use.

[0154] Preparation of Concave-convex Structure Layer Coating Solution

[0155]

[0156] Add 20kg of epoxy acrylate to 40kg of urethane acrylate, stir evenly, then add 25kgTPGDA and 15kgDPHA in turn, after stirring evenly, add 3kg 184 and 3kg TPO, stir well and prepare a concave-convex structure layer slurry for use.

[0157] Preparation of microcapsules and their dispersions

[0158] Preparation of oil phase solution:

[0159] 1-phenyl-1-dimethylphenylethane 60kg

[0160] CVL 1.5kg

[0161] BLMB 1.2kg

[0162] Trimethylolpropane adduct of hexamethylene diisocyanate 8kg

[0163] Methyl ethyl ketone 5kg

[0164] Add 1.5kg of CVL and 1.2kg of BLMB into 60kg of 1-phenyl-1-dimethylphenylethane and 5kg of methyl ethyl ketone, stir ...

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Abstract

The present disclosure relates to a chromogenic film and a pressure test film, the chromonic film comprising: a substrate on which other layers are coated to form a chromonic film; a concavo-convex structure layer formed on the substrate; and a chromonic film layer, which is coated on the concave-convex structure layer and contains microcapsules, which contain electron-donating leuco dye precursors, and the electron-donating leuco dye contacts electron-accepting compounds to be colored, wherein when the color develops When the film is pressed, the concave-convex structure layer presses the chromogenic layer, so that the microcapsules in the chromogenic layer are broken and released to the electronic leuco dye precursor. The chromogenic membrane realizes the narrowing and concentrating of the pressure-receiving area of ​​the pressure-testing membrane and the actual pressure-receiving area of ​​the microcapsules through the concave-convex structure layer, so even if a small pressure is applied to the pressure-testing membrane, the high sensitivity of the pressure-testing membrane can be realized.

Description

technical field [0001] The disclosure relates to a chromogenic film, a pressure test film and a preparation method thereof, in particular to a chromogenic film with a concave-convex structure layer, a pressure test film and a preparation method thereof. Background technique [0002] Pressure testing is mainly used in the lamination of printed circuit boards, confirmation and adjustment of pressure between rollers, lamination of liquid crystal glass panels, assembly of engine cylinders and other production and processing processes that have strict requirements on pressure. Pressure testing is usually performed with a pressure tester, but this pressure testing method is complicated to operate, has hysteresis in measurement results, poor test accuracy and sensitivity, and is only suitable for pressure testing in small areas, not suitable for online pressure monitoring, and not suitable Stress tests with specially shaped regions. [0003] To facilitate these pressure testing ap...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08J7/04C08J7/043C08L67/02C09D129/04C09D175/14C09D101/28C09D109/06C09D189/00C09D163/10C09D7/61G01L1/02
CPCG01L1/02C09D7/61C09D101/286C09D109/06C09D129/04C09D163/10C09D175/14C09D189/00C08J7/042C08J2367/02C08L2205/03C08L2205/035C08J2401/28C08J2409/06C08J2429/04C08J2489/00C08J2463/10C08J2475/14C08L9/06C08L63/10C08L67/02C08L29/04C08L89/00C08K3/34C08L75/14C08G18/69C08G18/0852C08G18/0857C08G18/73C08G18/7843C08G18/3206C08G18/3228C08J2409/08C08J2475/16C08J2375/14C08J5/18C08K9/10C09D7/41C09D7/70B05D7/02B05D7/536B05D3/067C08J2309/06
Inventor 崔叶冉光念刘亚军李亚想李娜曹雪杨茉杨伟闫志鹏
Owner BAODING LUCKY INNOVATIVE MATERIALS