High-temperature-resistant high-mineralization high-density water-based drilling fluid and application thereof
A water-based drilling fluid, high temperature resistant technology, applied in the field of drilling, can solve the problems of slow drilling speed, high cost, blowout, etc., and achieve the effect of good suppression
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[0016] In a second aspect, the present invention provides a method for preparing the high temperature resistant fluid loss control agent, the method comprising: in the presence of water as a solvent, a surfactant and an initiator, chlorinating dimethyl diallyl Ammonium, acrylamide, 2-acrylamido-2-methylpropanesulfonic acid, N,N-dimethylacrylamide and p-methylstyrene were polymerized.
[0017] In the method of the present invention, relative to 100 parts by weight of water, the amount of the surfactant can be 0.1-0.5 parts by weight, the amount of the initiator can be 8-12 parts by weight, the dimethyl The consumption of diallyl ammonium chloride can be 1-10 weight part;
[0018] In the method of the present invention, methyl diallyl ammonium chloride, acrylamide, 2-acrylamido-2-methylpropanesulfonic acid, N,N-dimethylacrylamide and p-methylstyrene The molar ratio of the amount used can be 1: (0.5-3): (1-5): (0.5-5): (0.5-4), preferably 1: (1.5-2.5): (3-5): (1 -3): (1-3).
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[0035] The present invention will be described in detail through examples below, but the present invention is not limited thereby. In the following preparation examples, examples and comparative examples, unless otherwise specified, the materials used are all commercially available, and the methods used are all conventional methods in the art.
[0036] Sulfonated lignite SMC, sulfonated lignite resin SPNH, sulfomethyl phenolic resin SMP-II and sulfonated asphalt were provided by China Petroleum Engineering Research Institute.
[0037] Polymer coating agent JT888, graphite and potassium chloride were purchased from Chengdu Chunfeng Petroleum Technology Co., Ltd.
[0038] Bentonite was purchased from Xinjiang Zhongfei Xiazijie Bentonite Co., Ltd.
[0039] The anti-high temperature fluid loss reducer is obtained according to the following preparation examples.
[0040] Dimethyldiallyl ammonium chloride, acrylamide, 2-acrylamido-2-methylpropanesulfonic acid, N,N-dimethylacrylami...
preparation example 1
[0043] In a three-necked flask equipped with a thermometer and a mechanical stirrer, dissolve 5g of 2-acrylamido-2-methylpropanesulfonic acid in 100g of deionized water, and , 2-acrylamido-2-methylpropanesulfonic acid, N,N-dimethylacrylamide and p-methylstyrene in a molar ratio of 1:2:4:2:2, add acrylamide in sequence , N,N-dimethylacrylamide, dimethyldiallylammonium chloride and p-methylstyrene, add 0.3g of sodium lauryl sulfate, adjust the pH of the solution to 7 with sodium hydroxide, and react After the device was sealed, it was flushed with nitrogen and stirred thoroughly, and 10 g of azobisisobutyramide hydrochloride with a mass concentration of 1% was added, and reacted at 50° C. for 6 hours to obtain a viscous liquid product. The obtained product was repeatedly purified with acetone, dried and pulverized at 100°C to obtain powdered high temperature resistant fluid loss reducer A1.
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