Method for extracting flavone by taking wild rough-peel mandarin as raw material
A technology for wrinkled citrus and wild citrus, which is applied in sampling, analysis materials, preparation of test samples, etc. It can solve the problems of limited raw materials, high cost, and difficult guarantee of product quality, and achieve low production cost, good product quality, The effect of good application prospects
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[0020] The method for extracting flavonoids from wild wrinkled mandarin oranges, the steps are:
[0021] 1. Raw material preparation: take the seven mature wild citrus oranges - wrinkled tangerines, peel them, wash them, chop them up, and dry them in an oven at 50° C., crush and sieve the dried citrus peels (40 mesh) to prepare Make citrus peel powder for later use.
[0022] 2. Extraction process: citrus peel powder→soaking→concentration under reduced pressure→dissolving with ethanol→constant volume
[0023] Weigh 30g of citrus peel powder, infiltrate with 60% ethanol as solvent according to the ratio of material to liquid 1:40, extract for 3 hours, extract at 50°C, then place the reactor in a microwave instrument, extract for 3-5min, and decompress Suction filtration to obtain the total flavonoids extract solution of wrinkled citrus peel, set the volume to 50ml, and set aside for testing.
[0024] 3. Determination of the content of flavonoids in the sample: taking rutin as ...
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